《High Efficient Extraction of Phthalates in Aquatic Products by a Modified QuEChERS Method》.pdfVIP
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Chem.Res.Chin.Univ.2013,29(4),653—656
EfficientExtractionofPhthalatesin Productsa
High Aquatic by
Modified Method
QuEChERS
WANG Zhen.boandLIU
Wen.wen,GAOFu.kai,LIGui.zhi,LIU Yong.ming‘
andChemical R.China
264005,P
CollegeofChemistry Engineering,YantaiUniversity,Yantai
AbstractA and efficientextractionmethodwas forthedetermina-
simple.environmentallyfriendlyhigh proposed
tionoffive in combinedwithmass detector
phthalatesaquaticproductsbygaschromatography spectrometry
thismethodwas were modified
(GC-MS).When adopted,samplespretreatedby
and toxic
effective,ruggedsafe)method.An
environmentallyfriendlyextractant(ethanolaqueoussolution)replaced
acetonitrilefor inthe ofbovineserum
extractingphthalatesprotein.matrixsamples.Fluorescencequenchingspectra
showthattherewasa interactionbetween and
albumin(BSA)withphthalates high.affinity phthalateprotein.de.
theextraction of fromfish the
80%(volumefraction,妒)ethanol
creasing efficiencyphthalates samples.However,in
slowbutfuU denaturationtakes wouldcausethe of andthe
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