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《235_ftp》.pdf
FULL PAPER
Nanostructuring Titania: Control over Nanocrystal Structure, Size, Shape,
and Organization
Abdelkrim Chemseddine*[a] and Thomas Moritz[b]
Dedicated to Professor J. Rouxel in recognition of his important contributions to the chemistry of solids
Keywords: TiO2 / Growth / Self-organisation / Polytitanate / Nanocrystals / Nanostructure / Superlattice / Films
Control over crystal structure, size, shape, and organization titania films. Furthermore, larger anatase TiO2 nanocrystals
of TiO2 nanocrystals has been achieved by means of wet of different sizes and shapes have been obtained by
chemistry. Hydrolysis and polycondensation of titanium adjusting the relative concentrations of titanium alkoxide
alkoxide [Ti(OR) ] has been performed in the presence of and Me NOH, the reaction temperature, and the pressure.
4 4
tetramethylammonium hydroxide (Me4NOH). This base both HRTEM, XRD, and EXAFS have been used to characterize
catalyzes the reaction and provides an organic cation that the various samples and to elucidate the growth of titania
stabilizes the anatase polyanionic cores formed in this anatase. Our observations are in accordance with
medium. These anatase clusters are organized so as to favour theoretically predicted condensation and growth pathways.
self-assembly into intermediate nanocrystals, which, in turn, The formation of mesoscopic structures through a self-
self-assemble into superlattices. This self-assembling process assemb
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