Rapid screening and identification of multi-class substances of very high concern in textiles using liquid chromatography-hybrid linear ion trap orbitrap mass spectrometry》.pdf
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Rapid screening and identification of multi-class substances of very high concern in textiles using liquid chromatography-hybrid linear ion trap orbitrap mass spectrometry》.pdf
Journal of Chromatography A, 1386 (2015) 22–30
Contents lists available at ScienceDirect
Journal of Chromatography A
j o u r n a l h o me p a g e : w w w. elsev /locate/chro ma
Rapid screening and identification of multi-class substances of very
high concern in textiles using liquid chromatography-hybrid linear
ion trap orbitrap mass spectrometry
Li Zhang a,b , Xin Luo b , Zengyuan Niu b,∗ , Xiwen Ye b , Zhixu Tang b , Peng Yao c
a College of Chemistry and Chemical Engineering, Ocean University of China, Qingdao 266100, China
b Inspection and Quarantine Technical Center, Shandong Entry-Exit Inspection and Quarantine Bureau, Qingdao 266002, China
c Key Laboratory of Marine Chemistry Theory and Technology, Ministry of Education, Ocean University of China, Qingdao 266100, China
a r t i c l e i n f o a b s t r a c t
Article history: A new analytical method was established and validated for the analysis of 19 substances of very high
Received 11 November 2014 concern (SVHCs) in textiles, including phthalic acid esters (PAEs), organotins (OTs), perfluorochemicals
Received in revised form 25 January 2015 (PFCs) and flame retardants (FRs). After ultrasonic extraction in methanol, the textile samples were ana-
Accepted 26 January 2015
lyzed by high performance liquid chromatography-hybrid linear ion trap Orbitrap high resolution mass
Available online 2 February 2015
spectrometry (HPLC-LTQ/Orbitrap). The values of LOQ were in the range of 2–200 mg/kg. Recoveries at
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