原创力文档《Synthesis and crystal Structure of 2[1-(1,1-dimethylethyl)-5-methyl-1-H-pyrazol-4-ylcarbonyl]-N-Phenyldrazinecarbothioamide》.pdfVIP
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《Synthesis and crystal Structure of 2[1-(1,1-dimethylethyl)-5-methyl-1-H-pyrazol-4-ylcarbonyl]-N-Phenyldrazinecarbothioamide》.pdf
23 卷4 期 结 构 化 学 JIEGOU HUAXUE Vol. 23, No. 4
2004. 4 Chinese J. Struct. Chem. 371~375
Synthesis and Crystal Structure of
2[1-(1,1-Dimethylethyl)-5-methyl-1-H-pyrazol-
4-ylcarbonyl]-N-phenyldrazinecarbothioamide
LI Minga, b, c WEN Li-Rongb FU Wei-Junb
ZHAO Gui-Longb YANG Hua-Zhenga
a (Institute of Elemento-organic Chemistry, Nankai University, Tianjin 300071, China)
b
(College of Chemistry and Molecular Engineering,
Qingdao University of Science and Technology, Qingdao 266042,China)
c (State Key Laboratory of Applied Organic Chemistry, Lanzhou University, Lanzhou 730000, China)
ABSTRACT The crystal structure of 2[1-(1,1-dimethylethyl)-5-methyl-1-H-pyrazol-4-ylcar-
bonyl]-N-phenyldrazinecarbothioamide ([C H N OS]CH COCH , C H N O S, M = 389.52)
16 2 1 5 3 3 19 27 5 2 r
has been determined by single-crystal X-ray diffraction. The crystal belongs to tetragonal, space
3
group I4 /a with a = 23.960(4), b = 23.960(4), c = 16.120(5) Å , V = 9254(4) Å , Z = 16, D = 1. 118
1 c
3 1
g/cm , m = 0.161 mm , F(000
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