原创力文档《Synthesis and Crystal Structure of 4-(2- Chlorophenyl)-5-cyano-3-methyl-6-oxo-1-phenyl-4,5,6,7-tetrahydropyrazolo[3,4-b] Pyridine under Microwave Irradiation》.pdfVIP
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《Synthesis and Crystal Structure of 4-(2- Chlorophenyl)-5-cyano-3-methyl-6-oxo-1-phenyl-4,5,6,7-tetrahydropyrazolo[3,4-b] Pyridine under Microwave Irradiation》.pdf
23 卷11 期 结 构 化 学 JIEGOU HUAXUE Vol. 23, No.11
2004.11 Chinese J. Struct. Chem. 1222~1225
Synthesis and Crystal Structure of 4-(2-
Chlorophenyl)-5-cyano-3-methyl-6-oxo-1-
phenyl-4,5,6,7-tetrahydropyrazolo[3,4-b]
Pyridine under Microwave Irradiation
ZHU Song-Leia, b TU Shu-Jianga LI Tuan-Jiea ZOU Xianga
ZHANG Xiao-Jinga JI Shun-Junc ZHANG Yongc
a (Department of Chemistry, Xuzhou Normal University,
Key Laboratory of Biotechnology on Medical Plant, Xuzhou, Jiangsu 221116, China)
b
(Department of Chemistry, Xuzhou Medical College, Xuzhou, Jiangsu 221002, China)
c (College of Chemistry and Chemical Engineering, Key Lab. of Org. Synth.
of Jiangsu Province, Suzhou University, Suzhou, Jiangsu 215006, China)
ABSTRACT The title compound (C H ClN O, M = 362.81) was synthesized by the reaction
20 15 4 r
of ethyl 2-cyano-3-(2-chlorophenyl)-1-acylate with 5-amino-3-methyl-1-phenylpyrazole under
microwave irradiation and its structure was determined by single-crystal X-ray diffraction. The
crystal is of monoclinic, space group P2 /n with a = 8.8192(19), b = 15.976(3), c = 13.094(3) Å , â
1
3 3 1
=
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