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Nucleation mechanisms and the elimination of misfit dislocations
at mismatched interfaces by reduction in growth area
E. A. Fitzgerald,a) G. P. Watson, R. E. Preano, and D. G. Ast
Department ofMaterials Science and Engineering, Cornell University, Ithaca, New York 14853
P. D. Kirchner, G. D. Pettit, and J. M. Woodall
IBM T. J. Watson Research Center, Yorktown Heights, New York 10598
(Received 15 August 1988; accepted for publication 18 November 1988)
To investigate the effect of growth area on interface dislocation density in strained-layer
epitaxy, we have fabricated 2-.um-high mesas of varying lateral dimensions and geometry in
4 2 2
(001) GaAs substrates with dislocation densities of 1.5 X 10\ 10 , and 10 cm-- • 3500-, 7000-,
and 8250-A-thick Ino (J5 Gao 95 As layers, corresponding to 5, to, and 11 times the experimental
critical layer thickness as measured for large-area samples, were then deposited by molecular-
beam epitaxy. For the 3500-A layers, the linear interface dislocation density, defined as the
inverse of the average dislocation spacing, was reduced from greater than 5000 to less than 800
em - I for mesas as large as 100pm. A pronounced difference in the linear interface dislocation
densities along the two interface (110) directions indicates that a dislocations nucleate about
twice as much as /3 dislocations. For samples grown on the highest dislocation density
substrates, the linear interface-dislocation density was found to vary linearly with mesa width
and to extrapolate to a zero linear interface-dislocation density for a mesa width of zero. This
behavior excludes dis
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