卫生杀虫微胶囊的研制及药效.pdfVIP

卫生杀虫微胶囊剂的研制及药效 摘要 本文用界面聚合法，以聚合MDI和多元胺为囊材，制备了农药微胶囊。着重探 讨了乳化剂用量、乳化速度、乳化时间、温度和反应时间等条件对微胶囊粒径和释 放速率的影响，得到了制备毒死蜱微胶囊的合适工艺条件，同时对分散剂、润湿剂、 增稠剂和防冻剂进行了筛选，测定了悬浮剂的相关参数，其包囊率达到93．2％，悬 浮率达到63％。采用相同工艺制备了2．5％毒死蜱·三氟氯氰菊酯微胶囊剂和2．5％ 三氟氯氰菊酯微胶囊剂，进行室内药效试验，在施药90d后，德国小蠊、致乏库蚊 和家蝇的死亡率仍可达到90％以上。微胶囊悬浮剂的原料成本仅为相应乳油原料成 本的一半。 关键词：毒死蜱；三氟氯氰菊酯；微胶囊；界面聚合法；室内药效；悬浮率 卫生杀虫微胶囊剂的研制及药效 TestsforIts ofPesticide and DevelopmentMicrocapsules EffectsOilHealthPests MDIand aswall interracial material，an Abstract：Usingpolymericpolyamine methodwasusedtomake reaction polymerization pesticidemicrocapsule．Several to sizesand were theeffects parametersparticle releasingcapacityinvestigated，including and of of time reaction time，reaction emulsifiers，emulsilyingrate，emulsifying quantity reactionconditionswere temperature．Optimum agent， andantifreezewereselected．Themain of agent parameterscapsulesuspension thickening weremeasured．Theratewas93．2％and rate to63％．2．5％ capsulate suspensibilitygot and were suspension chlorpyrifos＆cyhalothrincapsulesuspension2．5％cyhalothr／ncapsule withthesalIlemethodandreactionconditions．Theirtohealthwas made