原创力文档Effect of alcohol solvents treated ZrO（OH）2 hydrogel on properties of ZrO2 and its catalytic performance in isosynthesis.pdfVIP
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Effect of alcohol solvents treated ZrO（OH）2 hydrogel on properties of ZrO2 and its catalytic performance in isosynthesis.pdf
Availableonlineatwww．sciencedirect．c,om
． 一 ， ，
JOURNALOF
。：∥ScienceDirect NATURALGAS
CHEMISTRY
爱一 JournalofNaturalGasChemistry21(2012)1-6 www．elsevier．com／locate／jngc
EffectofalcoholsolventstreatedZrO(，OH、)，hydrogelonproperties
、 ， 一 - 一 一 一
ofZrO2anditscatalyticperformanceinisosynthesis
RongjunZhang，DehuaHe
InnovativeCatalysisProgram,KeyLabofOrganicOttoelectronicsandMolecularEngineering,
DepartmentofChemistry,TsinghuaUniversity,Bejiing100084,China
[ManuscriptreceivedAuguest15，2011；revisedOctober18，2011]
Abstraet
AseriesofZrO2catalystswerepreparedbytreatingZrO(OH)2hydrogelwithdifferentalcoholsolvents(C2一C4alcohols)andcalciningunder
N，flow at773K for3h．TheobtainedZr02catalystsweresystematicallychraacterizedbythemethodsofN2adsorption—desorption，powder
X—raydiffraction，NH3temperature—programmeddesorption，andCO2temperature—programmeddesorption．Thecatalyticperformanceofeach
catalystwasevaluatedintheselectivesynthesisofiso—C4(isobutenenadisobutane)nadlightolefins(c2~Ca)fromC0hydrogenation．The
specificsurfaceareaincreasedofrtheZrO2catalystsobtainedbytreatingZrO(OH)2hydrogelwithdifferentalcoholsolvents．Theamountsof
bothacidicnadbasicsitesonthe
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