毕业论文之完整.docVIP

本科毕业论文 本科毕业论文 市售奶茶粉中氟含量的测定 The sold Determination of Fluorine Content in the Milk Tea Powder 学 院：理学院 专 业：化学工程与工艺 学 号：081417475 姓 名：严红瑜 指导教师：赵智宏 职 称：副教授 论文提交日期：二〇一二年六月 摘 要 以市售奶茶为原料，本文采用沸水冲泡法和酸浸法两种方法，在pH值在5.5的条件下，用离子选择电极法测定奶茶中的氟含量，校准曲线回归方程为 E = 57.476lgCF-－237.2, (r2=0.9992)。方法的加标回收率在96.2%-103.5%之间，通过大量的奶茶中氟的测定,认为奶茶中酸溶性氟含量要比水溶性氟高，酸溶性氟含量更接近奶茶全氟含量。 关 键 词:奶茶；离子选择电极法；氟含量 The sold Determination of Fluorine Content in the Milk tea Powder Abstract With the sold milk tea as raw materials. Fluoride content of fluoride ion selective electrode method for the determination of tea, this paper uses two methods of boiling water method and acid leaching method , at pH 5.5 under the conditions of ion-selective electrode determination of fluoride content in tea, The calibration curve regression equation E = 57.476lgCF-－237.2 (r2 = 0.9992). Method of standard addition recoveries between 96.2% -103.5%, the determination of fluorine through a lot of tea, that the acid-soluble fluoride content in tea than water-soluble fluoride, acid-soluble fluoride content close to the total fluoride content of the tea. Key words: Milk tea; Ion Selective Electrode; Fluorine content 目 录 1 引言--------------------------------------------------------------1 1.1 研究的背景和意义----------------------------------------------1 1.2 目前测定氟含量的主要方法--------------------------------------1 1.3 本实验采用的方法----------------------------------------------1 2 实验部分----------------------------------------------------------2 2.1 实验原理------------------------------------------------------2 2.2 实验材料、仪器及试剂------------------------------------------2 2.2.1 样品来源-----------------------------------------------2 2.2.2 实验仪器-----------------------------------------------2 2.2.3 实验相关试剂-------------------------------------------3 2.3 实验方法------------------------------------------------------3 2.3.1 样品处理-----------------------------------------------3 2.3.2 测定方法--------------------------------