聂俊设计说明书概念.doc

学号： 常 州 大 学 毕业设计说明书 （2015届） 二○）设计工艺流程和工作步骤Process design of glycerol epichlorohydrin chlorination with 50,000 tons per year Abstract: The main task of the design is based on 95% of the raw material glycerine and 98% hydrogen chloride gas as a raw material in the Catalyst adipic acid catalytic synthesis of dichloropropanol (DCH), the chloride process technology design. Dichloropropanol (DCH) also called Dichloro glycerin, which is widely used, is the synthesis of epichlorohydrin (ECH) intermediates. It can also be used in the synthesis of acetate fibers, dichloroacetone, sewage treatment agent a variety of raw materials of chemical products. The design is based on the instructor given the mission statement on access to the relevant documents, completed the foreign language translation and literature review. In accordance with the requirements of the instructor to determine the design of the work program, under the teacher's guidance in determining the process, then the calculation and selection of material balance and heat balance of the chlorination process as well as the required process equipment design process and work steps. We prepared a manual calculation, design specifications, draw a diagram PID, PFD diagram, equipment layout plan and major equipment conditions Fig Finally, according to the selected device material, size and mass balance results, carried out equipment and raw materials investment estimation and simple technical and economic analysis, economic benefits derived project put into operation to meet the requirements of the basic chemical production plan. Key words: dichloropropanol; epichlorohydrin; chlorination; process design; intermediate; flowchart; material balance; heat balance; equipment selection; economic analysis 目 录 摘要 I Abstract II 1 总论 1 1.1设计目标 1 （1）设计题目 1 1.3设计的原则 1 1.4工厂设计地区及自然条件 1 1.5生产制度 3 1.6车间组成 3 2 文献综述 3 2.1.国内外环氧氯丙烷工业发展状况 3 2.1.1 国内状况 3 2.1.2 国外状况 4 2.2甘油法环氧氯丙烷工业发展前景 4 2.3环氧氯丙烷合成工艺路线简述 5 2.3.1丙烯