* In the second DSC thermogram the main reaction and decomposition are very close togather and hence if temperature control is not good then this reaction can easily go to undesirable decomposition. So DSC thermogram gives initial indication of how good a temperature control to be there and what margins you are having. * * TMR of 24hr is taken as relatively safer based on practical experience as one will have sufficient time take corrective action.As shifts are for 8hr anything less than would generally not acceptable. * * This can be derived experimentally based on DSC tests. * Based on the d
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