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3004铝合金退火工艺研究
Materials Science and Engineering A362 (2003) 274–279A study of annealing stages in Al– Mn (3004) alloy after cold rolling using positron annihilation lifetime technique and Vickers microhardness measurementsE. Gomaa a,?, M. Mohsen a, A.S. Taha b, M.M. Mostafa ca Physics Department, Faculty of Science, Ain Shams University, Abbasia, Cairo, Egyptb Metallurgy Department, Atomic Energy Authority, Nuclear Research Centre, P.O. 13759, Cairo, Egyptc General Organization of Import Export Control, Cairo Airport, Cairo, EgyptReceived 20 February 2003; received in revised form 9 July 2003AbstractPositron annihilation lifetime (PAL), scanning electron microscope (SEM) and Vickers microhardness (Hv) measurements have been performed to study the isochronal annealing of Al–Mn (3004) alloy in the temperature range from RT to 823 K after cold rolling at RT with various deformations of 7 and 23%. A positive correlation has been found between average lifetime (τav ) of positrons and Vickers microhardness.Three annealing stages of microstructures in Al–Mn (3004) alloy were distinguished which were attributed to recovery, partial recrystal-lization and complete recrystallization followed by grain growth. It appears that high cold work accelerated recystallization process while low cold work accelerated recovery process.? 2003 Elsevier B.V. All rights reserved.Keywords: Al alloys; Cold work; Recovery; Recrystallization; Positron annihilation lifetime; Vickers microhardness1. IntroductionPositron annihilation spectroscopy in particular positron lifetime (PAL) technique has been increasingly used to in-vestigate Al and Al alloys [1–8] . The combining analysis of microstructure aspect as given by PAL [9] with the micro-scopic characterization of the material through the measure-ment of the Vickers microhardness for commercial alloys of Al–Zn–Mg, showed the effects of the different ageing pro-cedures and how the chemical composition of the alloys, including secondary alloying elements may
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