《新建年产6万吨2_丙基庚醇车间合成工段工艺初步设计毕业设计》.docVIP

齐 齐 哈 尔 大 学毕业设计(论文)题目 年产6万吨2-丙基庚醇车间合成工段工艺初步设计学院化学与化学工程专业班级学生姓名指导教师成 绩2013 年 6 月日 摘 要 本年产6万吨2-丙基庚醇车间合成工段工艺初步设计。首先二丙基庚醇国内外现状，并简要介绍了二丙基庚醇的性质及方法其次介绍了课题的设计背景、厂址选择和原料产品规格；物料衡算、热量衡算对设备进行计算对自动控制、公用工程进行。最后根据毕业设计的要求利用AutoCAD绘制反应装配图合成工段设备平立面布置图手绘带控制点的工艺流程图完成20 000字的毕业设计说明书。 关键词：初步设计；合成工段； 2-丙基庚醇；衡算 The preliminary design of workshop of the synthesis section of 60,000 tons annual production capacity of 2-propyl heptanol was completed. Firstly, the significance, the function of 2-propyl heptanol, the development of research on 2-propyl heptanol was stated. The nature of 2-propyl heptanol and synthetic methods were described briefly. Secondly, the design background, plant location and materials and product specification were introduced; comparion of the productive processed in the domestic and aboard, the design process was determined. Meanwhile the material balance, heat balance, and the simulation of process by Aspen plus were finished. The reactor equipment and other major equipments were calculated and selected. And the layout of the equipment for the workshop, safety, environmental protection and public works were outlined. Thirdly, the equipments arrangement diagram of the workshop and the pentanal condensation reactor equipment assembly diagram were drawn with Auto CAD, the process flow diagram with control points was drawn by hand. Finally, the design instruction of 20 thousand words was finished. Key words：Preliminary designSynthesis section; 2 - propyl heptanol; Balance calculation目 录 摘 要 I Abstract II 第一章 总 论 1 1.1 概述 1 1.1.1 项目建设意义 1 1.1.2 国内外现状及发展前景 1 1.2 设计依据 3 1.3 厂址选择 4 1.3.1 厂址确定 4 1.3.2 厂址优势分析 4 1.4 设计规模与生产制度 5 1.4.1 设计规模 5 1.4.2 生产制度 5 1.5 原料和产品规格 5 1.6 经济核算 6 第2章 工艺设计和计算 7 2.1 工艺路线的选择 7 2.1.1 2-丙基庚醇工艺介绍 7 2.1.2 2-丙基庚醇工艺的确定 8 2.2 工艺流程简述 8 2.3 物料衡算 9 2.3.1 反应器R101的物料衡算 9 2.3.2 分离罐V103的物料衡算 10 2.3.3 换热器E101的物料衡算 11 2.3.4 精馏塔T101的物料衡算 11 2.3.5 换热器E104的物料衡算 12 2.3.6 反应器R102的物料衡算 12 2.3.7 换热器E105的物料衡算 14 2.3.8 闪蒸罐