制氢联合操作规程讲述.doc

山东东营海星化工有限公司 30000Nm3/h干气制氢及 10000Nm3/h甲醇裂解制氢装置 操 作 规 程 山东东营海星化工有限公司 2014年5月 范围 本规程主要规定了的工艺原理、流程、开停工操作法、岗位操作法及事故处理方案等内容。本规程适用于的生产操作。 引用标准 下列标准所包含的条文，通过在本中引用而构成本的条文。本出版时，所示版本均为有效。所有标准都会被修订，使用本的各方应探讨使用下列标准最新版本的可能性。 本规程起草单位：加氢改质车间 本规程于2014年5月开始编制 本规程负责编制人员：毛志伟、张国辉 车间复审：宋永明 公司审核：王刚 公司批准： 目 录 第一部分30000Nm3/h天然气转化制氢装置操作规程 第一章 装置概况 一 装置概述1 二 生产流程简述4 三 原料及产品的主要技术规格9 四 物料平衡11 五 装置消耗指标及能耗12 六 生产控制分析16 七 环境保护及安全措施29 八 装置对外协作关系23 第二章 制氢工艺原理 一 原料预加氢··········································24 二 原料脱硫与净化······································25 三 转化················································25 四 中温变换············································26 五 变压吸附············································27 第三章 装置正常操作 一 装置主要动设备操作法································28 二 脱硫精制系统操作法··································48 三 转化中变系统操作法··································56 四 锅炉系统操作法·······································73 五 PSA系统操作法·······································82 第四章 装置正常开工 一 开工前准备工作·······································109 二 气密···························110 三 脱硫系统升温开工····················113 四 转化中变催化剂还原···················116 第五章 装置正常停工与紧急停工 一 停工前准备工作·······································121 二 注意事项·············································121 三 停工步骤·············································121 四 装置紧急停工·········································122 第六章 事故处理 一 事故处理原则···········································125 二 重大事故处理方法·······································125 三 一般事故处理方法·······································125 第七章 安全技术 一 概述···················································128 二 氢气基本特性···········································128 三 系统的安全设施·········································128 四 消防···················································129 五 安全生产注意事项·······································129 附录一：30000Nm3/h天然气制氢流程图···························130 附录二：30000Nm3/h天然气制氢装置设备表·······················