experiment1-floridainternationaluniversity（1页）.docVIP

Forensic Chemistry Laboratory Manual Revision 7.1 Dr. Bruce McCord Department of Chemistry Florida International University Spring 2005 Laboratory Schedule Week 1 Footprints and Fingerprints 1 1a Week 2 Footprints and Fingerprints 2 1b Week 3 Seized Drugs: Spot tests 2a Week 4 Seized Drugs: microcrystal tests 2b Week 5 Seized Drugs: FTIR/UV/GC/ 2c Week 6 Documents and Trace: Inks by TLC 3a Week 7 Documents and Trace: Fibers by PLM 3b Week 8 Documents and Trace: Glass 3c Week 9 Explosives: Low Explosives 1 4 Week 10 Explosives: Low Explosives 2 4 Week 11 Toxicology:GC/MS 1 5 Week 12 Toxicology: GC/MS 2 5 Week 13 Arson 1 6 Week 14 Arson 2 6 Week 15 Presentation of Results 7 *Rotation Order Gr 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 1 1a 1b 2a 2b 2c 3a 3b 3c 4 4 5 5 6 6 mc 2 1a 1b 2a 2b 2c 3a 3b 3c 5 5 6 6 4 4 mc 3 1a 1b 2b 2a 2c 3b 3a 3c 6 6 4 4 5 5 mc 4 1a 1b 2b 2a 2c 3b 3a 3c mc Table of Contents Laboratory Procedures and General Information Footprints and Fingerprints Drug analysis: microscopic tests, color tests, and instrumental Trace Evidence: inks, paints and fibers Glass Analysis Explosives analysis: Spot tests, FTIR, Capillary electrophoresis Drug extraction in urine: GC/MS Arson analysis: GC-FID Appendix A, color test reagents ………………………………..………...46 Appendix B, Sample Lab Report…………………………………………….6 65 Notes 1. Each student will have one laboratory report for which the score will be thrown out 2. Removal from the labs or ingestion of controlled substances by any route, removal of equipment, glassware, and/or chemicals, cheating, dishonesty, plagiarism, or deception in fulfilling requirements will not be tolerated. Penalties include failing the course, and criminal prosecution. LABORATORY NOTEBOOK PROCEDURES The first page of the notebook should have your name and the course name. The second page of the notebook should be a table of contents. Each time an experiment begins, a page nu