Chemic的al oxygen demand automatic determination in high chlorine water by flow-injection analysis.docVIP

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Chemic的al oxygen demand automatic determination in high chlorine water by flow-injection analysis.doc

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Chemical oxygen demand automatic determination in high chlorine wastewater by high pressure flow-injection analysis (Chemical oxygen demand automatic determination in wastewater with high concentration of chloride by high pressure flow-injection analysis) Hong Ling-Cheng 1, Wang Lin-Qin 2 （1 Institute of Environment and Engineering, Hohai University, Nanjing, China, 210098 2 Delin Environmental Instrument Co.Ltd., Nanjing, China, 211103） Abstract：in this paper, an automated Chemical oxygen demand monitoring system has been developed.In the proposed system, Potassium dichromate in high temperature and high pressure of acidic dichromate, Therefore, the system was capable to determine Chemical oxygen demand in both the surface water with low Chemical oxygen demand concentration and the waste water containing up to 20000 mg Cl l-1 with the linear dynamic range of 0-10000 mg l-1 . The relative standard deviations were less than 2.1% and the quantification limit is as low as 4 mg l-1. The sampling frequency is 4-5 h-1,The most important is to recycle, avoid reagent for secondary pollution. Key words: Chemical oxygen demand; Flow Injection Analysis; Automatic;high chlorine;water Introduction Chemical oxygen demand (COD) represent the organic contaminants in water,which is frequently used as an indicator to identify the characteristics of wastewaters polluted mainly with organic compounds,is also the important parameters in water monitoring.To grasp the water quality situation,forecast water pollution accuratly,tracking pollution sources timely.In practical life, a fast, continuous and automatic method of COD determination is needed. The classic reference method for determination of COD[1-2] which is titration with potassium dichromate suffers from several disadvantages,such as the overall process is too long,large amounts of expensive and toxic chemicals are required,handling is also considerable, so the likelihood of errors is high and a skilled analyst is required. Bes