ppt课件-chapter_3c_ x_ ray_ diffraction.ppt（chapter_3c_间ray_ diffraction.ppt）.pptVIP

Crystal structure determination Monochromatic X-rays Panchromatic X-rays Monochromatic X-rays Many ?s (orientations) Powder specimen POWDER METHOD Single ? LAUETECHNIQUE ? Varied by rotation ROTATINGCRYSTALMETHOD As diffraction occurs only at specific Bragg angles, the chance that a reflection is observed when a crystal is irradiated with monochromatic X-rays at a particular angle is small (added to this the diffracted intensity is a small fraction of the beam used for irradiation). The probability to get a diffracted beam (with sufficient intensity) is increased by either varying the wave