《浙江师范大学-有机化学》化学-有机化学实验（一）1.docVIP

《有机化学实验(一)》课程实验教学大纲 一、课程概况（Course Outline） 课程名称：有机化学实验 (一) Course： Experiments in Organic Chemistry Ⅰ 课程编号： 0070300058 适用学生: 化学及应用化学专业 Course Number：Credit： 2 Workload: 72 Independent course：yes 预修课程： 无机化学实验 Prior Learning: Experiments in Inorganic Chemistry 二、课程简介 （Course Descriptions） 有机化学实验是一门独立的基础课程，由性质实验、基本操作实验、制备实验、设计性实验四部分组成。该课程目的在于训练学生基本操作技能，让学生掌握简单有机化合物的合成、纯化及结构测定方法；加深学生对化学基础理论、基本知识的理解，提高观察、分析和解决实际问题的能力，培养学生严谨的工作作风和实事求是的科学态度。 As an independent fundamental course, Experiments in Organic Chemistry includes four sections, identification of organic compounds, acquisition of basic laboratory skill, preparation of organic compounds, and design of organic experiments. Students are supposed to acquire the basic experiment skills and knowledge for preparation, purification, and identification of regular organic compounds. The course gives students a deeper understanding of fundamental experimental organic chemistry and exposes students to each technique in a systematic and in-depth way. Also, it trains students with the problem-solving ability as well as with strictness and scientific attitude. 三、实验项目一览表(Experiment List) 序号 No. 实验名称 Title 每组人数 Number of Students in each group 实验 时数 Hours 实验类型 验证∕综合∕设计 Experimental Type Characterization/Comprehensiveness /Designment 必做∕选做 Compulsory /Optional 1 仪器及实验室安全知识介绍 Introduction of Instruments and Safty Rules in Organic Chemistry Laboratory 1 4 验证 Characterization 必做 Compulsory 2 熔点测定 Determination of Melting Point 1 4 验证 Characterization 必做 Compulsory 3 蒸馏、沸点测定 Distillation and Determination of Boiling Point 1 4 验证 Characterization 必做 Compulsory 4 重结晶 Recrystallization 1 4 验证 Characterization 必做 Compulsory 5 水蒸气蒸馏 Steam Distillation 1 4 验证 Characterization 选做 Optional 6 折光率的测定 Determination of Refractive Index 1 4 验证 Characterization 选做 Optional 7 无水乙醇的制备 Preparation of Anhydrous Ethanol 1 4 验证 Characterization 必做 Compulsory