094103091012论文定稿精讲.docVIP

邯郸学院本科毕业设计 题 目 年产16万吨合成氨脱碳工段工艺设计 学 生 成亚杰 指导教师 梁亚男 讲师 年 级 2009级 专 业 应用化学 系 部 化学系 邯郸学院化学系 2013年6月  郑重声明 本人的毕业是在指导教师梁亚男的指导下独立撰写并完成的。毕业论文没有剽窃、抄袭、造假等违反学术道德、学术规范和侵权行为，本人愿意承担由此产生的各种后果，直至法律责任；并可以通过网络接受公众查询。特此郑重声明。 毕业作者： 年 月 日如不将其清除，在合成氨生产时CO2会使催化剂中毒。脱碳工段是合成氨工程中必不可少的工段之一3.6m，填料层高14m，下塔径为4.2m，填料层为9m。通过本设计方法，将原料气中的二氧化碳含量降低到1%以下，具有较好的脱出效果。附带的图纸带控制点的流程图和二氧化碳吸收塔设备结构图。 关键词 合成氨 脱碳工艺 热钾碱法 二氧化碳 The Design of 160kt/a Synthetic Ammonia Purification Section Process Cheng Ya-jie Driected by Lecturer LiangYa-nan Abstract It is an annual output of 160,000 tons of synthetic ammonia decarburization section in the design process. The carbon dioxide is harmful to ammonia synthesis catalyst, so it need removal of carbon dioxide in the feed gas, and it can be used for the production of other chemicals for example urea. It uses the developed way of hot solution of aqueous potassium carbonate and the process of two absorbtion and two recovery to remove the carbon dioxide of syngas, and to recover the carbon dioxide from the solution. The content of the design mainly includes the choice of the making technology, mass and energy balance, and the design of the equipments and tubes. The main equipment of this design is carbon dioxide absorption tower. The diameter of the upper part of the tower is 3600mm, height of the packing layer is 14m, diameter of the lower part of the tower is 4200mm and the height of the packing layer is 9m. In this way, to make the levels of carbon dioxide in feed gas be reduced to less than 1%, to meet the demand. The process flow chart with control points and synthesis tower assembly were drawn with CAD. Keywords Synthetic ammonia Decarburization process The hot solution of aqueous Technological design 目 录 摘　要 I 外文页 . II 1 前言 1 2　合成氨的概述 1 2.1 氨的发现与制取 1 2.2 氨的性质与用途 1 2.3 合成氨工业的发展现状 2 2.4 合成氨典型流程 2 2.5 脱碳在合成氨中的作用和地位 2 3　脱碳方法及工艺的选择 3 3.1 脱碳方法