低碳钢超声喷丸表面纳米化的研究.pdfVIP

第36卷第3期 2 0 0 0年3月 金属学坂 ACTA METALLURGICA SINICA V01．36 No．3 March 2 0 0 0 低碳钢超声喷丸表面纳米化的研究 木 冯淦，，z) 石连捷z) 吕坚s) 卢柯，) 1)中国科学院金属研究所快速凝固非平衡合金国家重点实验室，沈阳110015 2)南京理工大学材料科学与工程系，南京210094 3)LASMIS，University of Technology of Troyes，10000，Wroyes，France 摘要 利用超声喷丸技术在20低碳钢上制备出具有纳米晶体结构特征的表面层，利用x射线衍射及电镜分析研究了表面纳米层的微 观组织结构特征．结果表明，经超声喷丸处理可使样品表层晶粒细化至纳米量级．表层晶粒尺寸约为10 nm，微观应变为0．02％一0．04％． 表面纳米层厚度约为10 pm．另外，样品表层亚稳相Fe3C发生分解，形成纳米尺寸的石墨相和a—Fe相． 关键词 纳米晶体材料，表面纳米化，低碳钢，微观结构 中图法分类号TGl42．31，TGll3．1，TGll5．22文献标识码A文章编号0412一1961(2000)03—0300-04 INVESTIGj气TIoN oF SURFACE NANoCRYSTALLIZATIoN oF A LoW CARBoN STEEL INDUCED BY ULrrRASoNIC SHoT PEENING FENG Ganl固．SHI Lianjid)，L{)Jian3)．LU KeI) 1)State Key Laboratory for RSA，Institute of Metal Research，The Chinese Academy of Sciences，Shenyang 110015 2)Department of Materials Science and Engineering，Nanjing University of Science and Technology，Nanjing 210094 3)LASMIS，University of Technology of Troyes，10000，1Yoyes，France Correspondent：FENG Gan、Teh(02514315775 Manuscript received 2000--01--07 ABSTRACT A nanocrvstalline surface 1ayer was fabricated on a 20 steel plate by using an ultrasonic shot peening(USSP)technique．The USSP induced surface nanocrystallization products were characterized by means of XRD and TEM．Experimental evidences showed that after the USSP treatment for a short period of time．the initial coarse-grained structure in the top surface layer was refined into ultrafine grains．The mean grain size in the surface 1ayer iS about 10 nm and the mean microstrain about 0．02％～0．04％．The thickness of the nanocrystalline surface 1ayer is about 10肛m，which is dependent on the treatment duration． It was also found that the metastable phase Fe3 C in the surface layer decomposes into nanometer—sized graphite and Q—Fe phases after the USSP treatment． KEY WoRDS nanocrystalline material，surface nanocrystallization，low carbon steel，microstructure 金属纳米晶体材料由于其晶粒细小(通常小于100 nm)， 界面密度高，表现出独特的力学及物理化学性能【1。，为提高 传统材料的综合力学性能和服役行为开辟了新路．然而，尽 管目前已发展出多种纳米材料的制备技术，如金属蒸发凝聚 一原位冷压成型