食品包装用凝胶型二氧化碳指示标签研究.PDFVIP

包 装 学 报 Packaging Journal Vol.6 No.2 April 2014 第 6卷 第 2期 2014年 4月 食品包装用凝胶型二氧化碳指示标签研究 胡云峰 1, 2，陈君然 1，贺业鑫 1，胡晗艳 1，崔瀚元 2 （1. 天津科技大学 食品营养与安全省部共建教育部重点实验室，天津 300457；2. 天津市食品加工工程中心，天津 300457） 摘 要：在前期研究的基础上，以质量分数为 5%且质量之比为 3:2的甲基红和溴百里酚蓝混合溶液为 二氧化碳指示剂，甲基纤维素和甘油为主要成胶材料，制备了凝胶型二氧化碳含量指示标签。研究了凝胶 与指示溶液在变色过程中的吻合度，及运用该凝胶制备指示膜的最佳配方。研究结果表明：适量浓度甲基 纤维素制备的凝胶与指示溶液变色吻合度较高，对指示剂颜色变化无影响，可作为指示标签的主要成膜材 料；结合甲基纤维素凝胶的黏度、变色响应时间、挂壁百分比及流延性能等指标，确定出成胶的最适甲基 纤维素添加质量分数范围为 1.6%~1.8%；运用甲基纤维素质量分数为 1.6%~1.8%凝胶制备指示膜的过程中，适 宜的甘油添加量可以使成膜表面光滑、平整，并有利于水分的保持；最终确定指示标签的最佳制备条件为 甲基纤维素的添加质量分数为 1.8%，甘油的添加体积分数为 4%。 关键词：食品包装；二氧化碳；指示标签；凝胶 中图分类号：TS255.3 文献标志码：A 文章编号：1674-7100(2014)02-0027-07 Study on Gel-Type Carbon Dioxide Indicator Label Used in Food Packaging Hu Yunfeng1, 2, Chen Junran1, He Yexin1, Hu Hanyan1, Cui Hanyuan2 （1. Key Laboratory of Food Nutrition and Safety, Ministry of Education, Tianjin University of Science and Technology, Tianjin 300457, China; 2. Tianjin Food Engineering Center, Tianjin 300457, China） Abstract：On the basis of previous research, the gel-type carbon dioxide indicator label was studied. The indicator label consists of carbon dioxide indicator solution and gelling solvent. The mass concentration of the indicator solution was 5% and the indicator was composed of 3/5 methyl red and 2/5 bromothymol blue. Methyl cellulose and glycerol were the primary materials to make the gel. The goodness-of-fit during the color changing process of the gel and the indicating liquid were studied. Then the optimum formulation for the indicator film was studied by using the gel. Results show that: the gel made by appropriate concentration of methyl cellulose had a high goodness-of-fit with color change of indicator solution. As it had no effect on color change of indicator solution, so it could be used as the main film forming material to develop the indicator label. Considering overall indexes of viscosity, response time of color change, the hanging wall percentage and casting performance, the optimum