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Recycling of industrial solid waste for the removal of mercury (II) by adsorption process.pdf

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Recycling of industrial solid waste for the removal of mercury (II) by adsorption process

Pergamon Chemosphere, Vol. 34, No. 2, pp. 357-375, 1997 Copyright Q 1997 Elsevier Science Ltd Printed in Great Britain. All rights reserved HI: SOO45-6535(96)00383-9 0045-6535/97 $17.00+0.00 RECYCLING OF INDUSTRIAL SOLID WASTE FOR THE REMOVAL OF MERCURY II) BY ADSORPTION PROCESS C.NRMASIVAYAM* and S.BENTHILKUMAR Environmental Chemistry Division Department of Environmental Sciences Bharathiar University. Coimbatore - 641 046 Tamil Nk, INDIA ABSTRACT (Received in USA 16 May 1996; accepted 25 August 1996) Pe(II1) / CrIII) hydroxide, a waste byproduct obtained fro5 the treatrent of Cr(V1) containing wastewaters in a fertilieer industry, has been used for the adsorption of I(11) fro5 aqueous solution. The influence of various parameters such as retal ion concentration ( 10 - 48 sg/L), agitation tire (1 - 160 sin), adsorbent dosage (5 -258 sg per 50 511, tesperature (24 - 44 C) and pH value (4 - 10) on the reroval of Hg(I1) has been studied. The adsorption follone both Laugsuir and Freundlich isotherr rodels. The applicability of the Lsgergren kinetic rode1 has been investigated. Alrost quantitative reroval of Hg(I1) fro5 a solution containing 48 sg/L in a 563 rl solution by 175 sg of adsorbent occurred at au initial pH of 5.0. Adsorption was uniforraly high (91 X) in the initial pH range 4.0 to 1B.H. Tesperature studies showed that the adsorption process was endotherric in nature. Desorption of Hg(II) showed that it is aolubilieed in 2 X KI to the extent of 65 X. 0 1997 Elsevier Science Ltd. All rights reserved Key words : Waste Fe(II1) / Cr(II1) hydroxide, HCI(II) adsorption. isotherrs, kinetics. -_-_----___________-~~~~~~~~~~~~~~~~-~-~~~-~~~~~~-------------~--~~- 5 Author to who5 oorrespondence should be addressed E-mail: sandyBas250.bharathi.ernet.in 351 358 INTRODUCTION The m,jor sources of mercury pollution in the aquatic environment are industries such as chloralkali, paint, electrical, rubber processing, oil refining and fer