白桦树皮单宁的微波辅助提取工艺研究.pdfVIP

现代农业科技 2013 年第 1 期 资源与环境科学 白桦树皮单宁的微波辅助提取工艺研究 曹一技 l 刘永 1.2 张德辉 l 丁为民 1.3 王洋 1 事 (东北林业大学盐碱地生物资源环境研究中心东北油田盐碱植被恢复与重建教育部重点实验室，黑龙江哈尔滨 15ω40; 2 黑龙江出入境检验检 疫局; J 哈尔滨理工大学化学与环埠工程学院) 摘要 白桦是一种重要的林木资源。研究了白桦树皮中羊宁的微波辅助提取工艺，确定了最佳工艺条件。微波辅助提取桦树羊宁的最 佳条件为:在乙醇浓度为 33 %(VfV)，提取时间为 928 、提取温度为 80 c、微波功率为 75W 的条件下，微波辅助提取桦树单宁的收率达到 5.61% ，纯度为 5 1.1 8% 。 关键词 白桦;树皮;单宁;均匀设计;微波辅助;提取工艺 中图分类号 TQ654.2; TQ284.23 文献标识码 A 文章编号 1 ∞7-5739(2013 )01-02 11 -02 Study on the Microwave-assisted Extraction Technology of Tannin from Bark of Betula p缸纱Phylla CAOYi-bo l LIDYo吨 1.2 ZHANG De-hui 1 DING Wei-min 1.3 W ANG Yang 1* (IAlkali Soil Natural Environmental Science Center, Northeast Forestry University , Key Lahoratory of Saline-a1kali Vegetation Ecology Restoration in Oil Field(Mini8lry ofEducation) , Harbin Heilongjiang 15∞40 卢 Heilongjiang Entry-exit Inspection and Quarantine Bureau; 3Sc hool of Chemical and Environmental Engineeri吨， Harbin University of Science and Technology) Abstract Retu1a platyphylla was one of the important biomaterial resources. Microwaves-assisted extraction of tannins from bark of Betulα p/I/1Jphylla were optimized ,,,ing uniform d四ign. TI.e optimal conditione were 33% alcohol( vfv) 臼 the extraction solvent. 92 吨 as the èxlrafliflll time , 80 吨~ as the extra正地 iutl temperatw毡， 75 W ofmicrowave power.Tannin yield could reach up to 5.61% with the purity of5 1. 18 1毛 under above conditions. Key words Betula plalyphylla; bark ; tannin; uniform design methodology; microwave-皑白时; extraction technology 白桦 (Betulapl，ωyphylla) 是黑龙江省重要的林木资源 [1] 。 树皮粉碎后过筛，备