原创力文档Control synthesis of rutile TiO2 microspheres, nanoflowers, nanotrees and nanobelts via acid-hydroth.pdf
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Control synthesis of rutile TiO2 microspheres, nanoflowers, nanotrees and nanobelts via acid-hydroth
Dynamic Article LinksCCrystEngComm
Cite this: DOI: 10.1039/c1ce05186e
/crystengcomm PAPER
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View OnlineControl synthesis of rutile TiO2 microspheres, nanoflowers, nanotrees and
nanobelts via acid-hydrothermal method and their optical properties?
Weijia Zhou, Xiaoyan Liu, Jingjie Cui, Duo Liu, Jing Li, Huaidong Jiang, Jiyang Wang* and Hong Liu*
Received 9th February 2011, Accepted 1st April 2011
DOI: 10.1039/c1ce05186eSemiconductor rutile TiO2 nanostructures with a diversity of well-defined morphologies, such as
microspheres, nanoflowers, nanotrees and nanobelts, are synthesized via an acid-hydrothermal process
without any structure-directing agents. Their morphologies, crystal structures and orientation
relationship were characterized by X-ray diffraction, scanning electron microscopy and high-resolution
transmission electron microscopy. By controlling hydrochloric acid concentration, anisotropic growth
of the rutile TiO2 leads to various morphologies. The synthesis mechanism of rich TiO2 nanostructures
was also studied. Finally, the relationship between optical properties and the structural complexity of
the rutile TiO2 nanocrystals was characterized.Introduction
Design and growth of inorganic nanostructures with controlled
size and morphologies has been the focus of intensive research on
both relevant theories and technologies in recent years owing to
the wide range of electrical and optical properties.1–4 Chemical
vapor deposition (CVD),5 application of templates,6 catalysts7
and electrochemical methods8 are general synthesis routes to
direct the growth of inorganic material with controlled
morphologies and architectures. In addition to the above
methods, the simple solution synthesis approaches by hydro-
thermal treatment have become a promisin
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