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Electroless-plated tin compounds on carbonaceous mixture as anode
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dJournal of Power Sources 193 (2009) 810–815
Contents lists available at ScienceDirect
Journal of Power Sources
journa l homepage: www.e lsev ier .com/ locate / jpowsour
lectroless-plated tin compounds on carbonaceous mixture as anode
or lithium-ion battery
i Ruei Jhana, Jenq Gong Duha,?, Mo Hua Yangb, Deng Tswen Shiehb
Department of Material Science and Engineering, National Tsing Hua University, Hsinchu, Taiwan
Material and Chemical Research Laboratories, Industrial Technology Research Institute, Hsinchu, Taiwan
r t i c l e i n f o
rticle history:
eceived 8 September 2008
eceived in revised form 9 March 2009
ccepted 31 March 2009
vailable online 16 April 2009
eywords:
n
a b s t r a c t
A composite anode materials was prepared that contained tin compounds of Sn6O4(OH)4, SnO2 and
Sn3PO4 on the surface of carbonaceous mixture mesophase graphite particles (MGP) and nature graphite
(NG). The nanosize tin compounds were electrolessly plated from aqueous solutions onto the carbona-
ceousmixture. Themorphology and structure of tin compoundswere characterized by scanning electron
microscopy (SEM) and X-ray diffraction (XRD). It was found that the tin compounds particle size was a
crucial factor to improve Sn compounds/Carbon composite anodes for cyclability and reversible capacity.
The homogeneous dispersion and smaller particle size of tin compoundswas attributed to the additive of
NG. As the carbonaceous substrate was C–Cmixture carbon, the particle size of Sn compounds was aboutarbonaceous mixture
omposite anode
lectroless plating
ithium-ion batteries
20–30nm.However, the particle sizewas 100–200nm, as the carbon substratewas singularMGP. Electro-
chemical performance test of the Sn compounds/C–C composite electrode shows the maximum specific
charge capacity of 583mAhg?1 at the 5th cycle. The charge capacity retention of Sn compounds/C–C
electrode was 85% after 20 cycles. The reversible capacity of Sn
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