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Mechanisms of phosphorus removal by cement-bound ochre pellets.pdf

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Mechanisms of phosphorus removal by cement-bound ochre pellets

Chemosphere 90 (2013) 1533–1538Contents lists available at SciVerse ScienceDirect Chemosphere journal homepage: www.elsevier .com/locate /chemosphereTechnical Note Mechanisms of phosphorus removal by cement-bound ochre pellets James Littler a, Jennifer N. Geroni a,?, Devin J. Sapsford a, Richard Coulton b, Anthony J. Griffiths a aCardiff University, School of Engineering, Cardiff CF42 3AA, UK b Siltbuster Ltd., Unipure House, Wonastow Road, Monmouth NP25 5JA, UK h i g h l i g h t s Quantification of P-removal by acid mine drainage (AMD) ochre and cement-bound ochre. P-removal enhanced in ochre pellets compared to unbound solids. Enhanced P-removal predominantly attributable to cement binder, not ochre. P-removal largely a result of hydroxyapatite (HAP) precipitation.a r t i c l e i n f o Article history: Received 6 May 2012 Received in revised form 26 August 2012 Accepted 27 August 2012 Available online 3 October 2012 Keywords: Ochre pellets Cement Hydroxyapatite precipitation Phosphorous removal0045-6535/$ - see front matter 2012 Elsevier Ltd. A /10.1016/j.chemosphere.2012.08.054 ? Corresponding author. Tel.: +44 (0)79 E-mail address: geronijn@cf.ac.uk (J.N. Geroni).a b s t r a c t Hydrous ferric oxide (here termed ‘ochre’) sludge, an abundantwaste product produced from the treatment of acidminedrainage (AMD),wasused in this study for the removal of phosphorus (in the formofphosphate ions) from contaminated waters. The phosphorus uptake capacities of both raw and pelletized AMD solids were compared using batch and column tests. Addition of a cement binder to the AMD solids during pellet production led to significantly increased P-loading of the resultant solids compared to the rawsludge. Addi- tionally, the pellets were found to continue to remove P in tests up to 7 d in duration whereas the unbound AMDsludge appeared to approach equilibriumwith phosphate solution after approximately 60 minof con- tact time. In linewith previous studies P uptake by