37 Salvia particle fingerprint characteristics of.docVIP

 PAGE \* MERGEFORMAT 10 37 Salvia particle fingerprint characteristics of Author: Zhang Lihua Yuan Guang Xin Zhao Lili Jia Dewei [Abstract] Objective: To establish a 37 Danshen particles HPLC fingerprint characteristics of quantitative and qualitative TLC map. Methods: TLC method, 37 particles in the main component of Danshen 37 for qualitative identification; 37 Danshen using HPLC determination of B particles in the acid content of Denmark. Results: TLC characteristic pattern can be clearly detected in 37; HPLC method measured the characteristics of this product in the map to determine the content of Sal B. In 0.02068μ g ~ 2.585μ g within the framework of solution concentration and peak area showed good linear relationship, r = 0.9999, average recovery was 98.47% (n = 5), RSD 1.8%. Conclusion: The fingerprint features patterns can be accurately and quickly to carry out qualitative and quantitative detection, can be used for the preparation of the internal quality control. [Keywords:] 37 Salvia particles TLC HPLC method Sal B Study on Sanqi danshen granula by finger-print differentiation [Abstract] Objective: to set up quantitative measure of SQDSG by HPLC method and qualitative specific fingerprint spectrum of TLC.method: to differentiate qualitatively the main gradients sanqi / danshen to SQDSG; to measure the content of danfensuanB by HPLC METHOD.Result: sanqi can be detected dramatically by TLC specific chromospectrum; content of danfensuanB can be determined by specific fingerprint spectrum woth HPLC method, and concentration of n conternt by HPLC method, shows a good linear relation with peak area, ranging form 0.02068μ g ~ 2.585μ g, r is 0.9999, the average retrieve rate is 98.47 (n = 5), RSD is 1.8%. concusion: the characteristic fingerprint spectrum is a rapid and accurate method for quantitative and qualitative measurement for internal control of the preparation. [Keywords:] sanqi danshen granula (SQDSG); single layer differentiation; HPLC met