Chuanxiong quality standards of.docVIP

 PAGE \* MERGEFORMAT 11 Chuanxiong quality standards of [Abstract] Objective Chuanxiong method of identifying perfect Chuanxiong quality standards. Methods TLC identification Chuanxiong to Determination of ferulic acid. Selection of Agilent Eclipse XDB-C18 column (4.6 mm × 150 mm, 5 μm), mobile phase was methanol -1% acetic acid solution (21:79), flow rate 1.0 mL / min, detection wavelength was 320 nm. the results of the TLC spots were clear and easy identification. High liquid chromatography precision, reproducibility, and ferulic acid 0.042 5 ~ 0.382 5 μg in the range a good linear relationship, the average recovery was 97.10% (RSD = 1.31%). Conclusion The method can effectively Control Chuanxiong quality. [Keywords:] Chuanxiong, TLC; high performance liquid chromatography, quality standards Abstract: Objective To improve the quality standard for Chuanxiong by studing the method of discriminating Chuanxiong. Methods Chuanxiong was identified by TLC. The content of ferulic acid in Chuanxiong was determine by HPLC. The Agilent Eclipse XDB-C18 (4.6 mm × 150 mm, 5 μm) was used, mobile phase was methanol-1% acetic acid solution (21:79), flow rate was 1.0 mL / min, detection wavelength was 320 nm. Results The TLC spots developed were fairly and simply identical. HPLC was accurate and reproducible. Ferulic acid showed a good liner relationship at range of 0.042 5 ~ 0.382 5 μg, the average recovery was 97.10% (RSD = 1.31%). Conclusion These methods can be used to control the quality of Chuanxiong effectively. Keywords:: Chuanxiong, TLC, HPLC, quality standard Chuanxiong is commonly used Chinese medicine for the treatment of irregular menstruation, dysmenorrhea, amenorrhea, Xiong Xie tingling Fengshibitong and so on. lt;lt;Chinese Pharmacopoeiagt;gt; have used properties, microstructure, TLC medicines to control chuanxiong quality. In order to quality control standards Chuanxiong more scientific, rigorous testing and more adapted to modern technology, I