Citrus aurantium in microwave-assisted extraction of active ingredients of naringin.docVIP

 PAGE \* MERGEFORMAT 11 Citrus aurantium in microwave-assisted extraction of active ingredients of naringin Of: Wang Guihua, Zhou Feng, Zhao Changqing, Yang Yi, Fang Jing, Guo Library [Abstract] Objective To establish the ethanol in the microwave-assisted extraction of naringin in Citrus aurantium extract. Methods were investigated by orthogonal experiments of ethanol concentration, microwave power, microwave extraction and liquid-solid ratio and time on the extraction of naringin in Citrus aurantium effect. The results obtained optimized microwave extraction conditions: 40% ethanol, microwave power 425 W, liquid to solid ratio 50 ml / g, microwave extraction time was 4 min. Under the optimum conditions, were The average recovery experiment, recovery was 96.8% ~ 102.4%, RSD 2.57%. Conclusion Orthogonal active ingredients out of naringin in Citrus aurantium in the microwave extraction process is reasonably practicable, microwave assisted extraction and Soxhlet extraction , ultrasonic extraction method compared with the fast, efficient and so on. [Keywords] microwave assisted extraction, Citrus aurantium, naringin Abstract: ObjectiveTo establish a microwave-assisted extraction (MAE) method for the extraction of the naringin in Fructus Aurantii. MethodsVarious experimental conditions of MAE affecting extraction of naringin from Fructus Aurantii were investigated by orthogonal experiments, such as ethanol concentration, the microwave power, the liquid / solid ratio and the microwave-extraction time.ResultsThe optimum conditions of MAE were obtained: ethanol concentration 40%, the microwave power 425W, the liquid / solid ratio 50 ml g-1, the microwave-extraction time 4 min. With the optimized condition, the recoveries were from 96.8% to 102.4% and relative standard deviation (RSD) was 2.57%. ConclusionMAE for effective constituent from Fructus Aurantii by orthogonal experiments is suitable and feasible. Compared with Soxhlet extraction and Ultrasonic ex