Cynanchum komarovii grass Purification and characterization of the active ingredient.docVIP

 PAGE \* MERGEFORMAT 8 Cynanchum komarovii grass Purification and characterization of the active ingredient [Abstract] Objective AB  8 macroporous resin Cynanchum komarovii grass in the extraction and separation of effective components. Methods macroporous resin column chromatography, silica gel column chromatography and recrystallization to extract Cynanchum komarovii grass in the active ingredients. The results of the isolated compounds using mass spectrometry, infrared spectra, UV spectra were characterized by Cynanchum komarovii grass proved to be the active ingredients. Conclusion Cynanchum komarovii grass in the active ingredients can be AB  8 macroporous resin into the separation. [Keywords:] Cynanchum komarovii grass; the active ingredient; macroporous resin; Structural Characterization Cynanchum komarovii grass Cynanchum komarovii Al. Iljinski is dry sand area in northwest China are widely distributed herbs [1]. The study found that extract of Cynanchum komarovii anti-inflammatory, antibacterial, anti-tumor and analgesic effect, with a strong biological activity [2,3]. In particular, its total alkaloids in the 7 - de-Methoxy Tylophora base pairs of tobacco mosaic virus (TMV) has a strong inhibitory effect, more than today’s generally accepted anti-plant virus inhibitors. Cynanchum komarovii grass as a plant pesticide belonging to biological categories of natural plant-based anti-virus inhibitors, as well as the promotion of Combined effects of plant growth [4], but because of its difficult extraction and separation of active ingredients. Therefore, it is difficult extraction process used in its production. In order to explore the industrialized Cynanchum komarovii grass extract the active ingredients in the process route, the research group studied the use of macroporous resin adsorption and separation of Cynanchum komarovii grass alkaloid extract of the method and conditions of [5]. In this paper, the chosen AB-8 macroporous adsorption resin ex