网站大量收购独家精品文档,联系QQ:2885784924

Preconcentration flow injection cold vapor atomic absorption fluorescence spectrometry of trace inorganic mercury in mineral water.doc

Preconcentration flow injection cold vapor atomic absorption fluorescence spectrometry of trace inorganic mercury in mineral water.doc

  1. 1、本文档共14页,可阅读全部内容。
  2. 2、原创力文档(book118)网站文档一经付费(服务费),不意味着购买了该文档的版权,仅供个人/单位学习、研究之用,不得用于商业用途,未经授权,严禁复制、发行、汇编、翻译或者网络传播等,侵权必究。
  3. 3、本站所有内容均由合作方或网友上传,本站不对文档的完整性、权威性及其观点立场正确性做任何保证或承诺!文档内容仅供研究参考,付费前请自行鉴别。如您付费,意味着您自己接受本站规则且自行承担风险,本站不退款、不进行额外附加服务;查看《如何避免下载的几个坑》。如果您已付费下载过本站文档,您可以点击 这里二次下载
  4. 4、如文档侵犯商业秘密、侵犯著作权、侵犯人身权等,请点击“版权申诉”(推荐),也可以打举报电话:400-050-0827(电话支持时间:9:00-18:30)。
查看更多
Preconcentration flow injection cold vapor atomic absorption fluorescence spectrometry of trace inorganic mercury in mineral water

 PAGE \* MERGEFORMAT 14 Preconcentration flow injection cold vapor atomic absorption fluorescence spectrometry of trace inorganic mercury in mineral water Of: Zi Hong Jinggan fifty-two Hansu Ping Jiang Xianjuan Ling in the end [Abstract] of the PTFE tube knotted reactor (KR-line sorption preconcentration and cold vapor atomic fluorescence technology combined with determination of trace inorganic mercury mineral water method. Hg2 + and Hg2 + DDTC DDTC-line complex formation and adsorption the inner walls of the KR, the use of electromagnetic induction heating technology, with 20% (V / V) HNO3-line pre-heated elution and oxidation on the inner wall enriched in KR Hg2 + DDTC. eluent solution and the reaction KBH4 mercury vapor, direct associated with cold vapor atomic fluorescence was detected by .20% (V / V) HNO3 as the eluent at the same time provide a place for the hydrogenated acid medium. This method does not use a common organic eluent with a simple operation and environmental protection advantages. Analysis of 30 samples per hour, maximum adsorption ratio of 35 times, sample analysis precision RSD was 2.2% (n = 11), the detection limit (3σ) was 2.0 ng / L. [Keywords:] knotted reactor, electromagnetic induction heating, cold vapor atomic fluorescence spectroscopy, inorganic mercury, mineral water Abstract Flow injection on line sorption preconcentration and separation in a knotted reactor (KR) was coupled to cold vapor atomic fluorescence spectrometry for the determination of trace mercury in mineral water. Mercury was preconcentrated by on line formation of mercury diethyldithiocarbamate complex (Hg DDTC) and absorption of the resulting neutral complex on the inner walls of a knotted reactor. A 20% (V / V) HNO3 solution heated by electromagnetic induction heating technique was used as eluent to remove the absorbed Hg DDTC from the KR, and then the vapor mercury generated by mixing the resulting solution and KBH4 was determined on line by cold va

文档评论(0)

hhuiws1482 + 关注
实名认证
内容提供者

该用户很懒,什么也没介绍

版权声明书
用户编号:5024214302000003

1亿VIP精品文档

相关文档