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Qin Bo compound granules Extraction Process
PAGE \* MERGEFORMAT 9
Qin Bo compound granules Extraction Process
[Abstract] By means of rhubarb, Corydalis comparison of thin-layer chromatography, and the pairs of berberine, baicalin contents were determined reference points better than the mixed formulation. And using orthogonal experiment investigated soaking time, add water, add alcohol volume, extraction time and ethanol concentration of several factors to determine the water extraction and alcohol extraction process conditions.
[Keywords:] baicalin and berberine fractionation mention orthogonal mixed
Qin Bo compound granules from Scutellaria, Phellodendron, rhubarb composed of 11 Chinese herbal medicines. Hemorrhoids surgery for clinical infection, results were satisfactory. In order to fully make the active ingredients in medicinal herbs to improve the quality of preparation, this extraction process of the preparation of the system studies.
An instrument and reagent
1.1 Instrument Shimadzu CS-930 dual wavelength TLC scanner, micro-injector (10ul) (Shanghai Medical Laser Instrument Factory). uv-1 type three UV analyzer, CX-100 ultrasonic cleaner.
1.2 reagent anhydrous ethanol, methanol, 95% ethanol, benzene, chloroform, formic acid, acetic acid, ethyl acetate, n-butanol, etc. are AR, berberine, baicalin (Ministry of Health, pharmaceutical and biological products Office).
Extraction of the choice of two routes
The preparation prescribed by the 11 Chinese herbal medicines, of which Mr Wong, Gentiana, Xuan Hu, betel nut inclusive of alkaloids, the active ingredient of Alisma triterpenoids, soluble in organic solvents. Which rhubarb, angelica, wind, habitat, peach seed, Scutellaria baicalensis active ingredient can be dissolved in water. Compounded by Rhubarb, Scutellaria baicalensis and other traditional Chinese medicine active ingredients in acidic, while the alkaloid was alkaline, acid and alkali-prone response to precipitation, thus affecting the leaching of which the active ingredient. To this
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