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RP-HPLC determination of puerarin in neck-pass particle content of
PAGE \* MERGEFORMAT 11
RP-HPLC determination of puerarin in neck-pass particle content of
【Abstract】 Objective RP-HPLC (RP HPLC) determination of carotid-pass particles in the content of puerarin. Methods Dima RP 18 (4.6 mm × 150 mm, 5 μm), mobile phase: methanol -0.025 mol * L-1 phosphoric acid (20:80), detection wavelength λ = 250 nm, column temperature 30 ℃, flow rate 1 ml / min. The results of puerarin was 0.005 ~ 0.05 mg / ml concentration range a good linear relationship, (r = 0.999 9). The average recovery of 100.23%, RSD = 1.35% (n = 5). Conclusion The method is simple, reliable, good reproducibility can be used as drug quality control methods.
Keywords: puerarin; neck-pass particle; RP-HPLC
Determination of Puerarin in Jingtong Granule by RP-HPLC
Abstract: ObjectiveTo establish an RP-HPLC method for determination of puerarin in Jingtong Granules. MethodsDIKMA RP-18 column (4.6mm × 150mm, 5μm) was used with methanol-0.025mol / L phosphoric acid (20:80) as a mobile phase . The detection wavelength was set at 250 nm.The temperature of column was at 30 ℃, and flow rate was 1.0 ml / min.The injection volume was 20μl. ResultsThe linear relationship of puerarin was good in the range of 0.005 ~ 0.05μg / ml (r = 0.999 9). The average recovery was 100.23%, RSD = 1.35% (n = 5). ConclusionThis method is simple and credible. It can be used for the quality control of Jingtong Granules.
Keywords:: Puerarin; Jingtong Granules; RP-HPLC
Neck-pass particles by the TGP, puerarin, Clematis, Codonopsis, Astragalus, etc. 12 flavor processed into Chinese herbal medicine is extracted with nourishing Qi, promoting blood circulation, scattered wind analgesic effect. For neck pain caused by cervical spondylosis, activities difficult, back pain, upper limb numbness, or muscle atrophy embolism. Puerarin its main active ingredient. Is intended to liquid chromatography puerarin content in the appropriate chromatographic conditions fo
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