立板式隔板塔分离直馏汽油工艺.pdfVIP

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立板式隔板塔分离直馏汽油工艺

学兔兔 化 工 进 展 2009年第28卷第8期 CHEMICAL INDUSTRY AND ENGINEERn G PROGRESS ·1337· 立板式隔板塔分离直馏汽油工艺 朱怀工 ,-,王 燕 ,张敏卿 ( 天津大学化工学院,天津300072; 中国吴华天大天久科技股份有限公司,天津300072) 摘 要:对利用一种新型立板式隔板精馏塔切割直馏汽油工艺进行了研究。首先,利用模拟软件HYSYS对该分 离过程进行模拟,得到较优的工艺条件。在此基础上,利用立板式隔板塔实验装置,考察了塔顶总回流量、液体 分配比等操作参数对产品的影响及装置的操作稳定性。结果表明,塔顶总回流量的增大有助于产品的分离,且液 体分配比的选择范围更广。液体分配比的改变对中间侧线产品质量的影响较大,是操作的关键变量。 关键词:立板式隔板塔;完全热耦合;直馏汽油;分离 中图分类号:TQ 028.8 文献标识码:A 文章编号:1000—6613(2009)08—1337—06 Straight-run gasoline separation with dividing wall column ZHUHuaigong1’。,WANG Yan ZHAN GMinqing2 , ( School of Chemical Engineering and Technology,Tianjin University,Tianjin 300072,China; Haohua Univtech Co Ltd.,Tianjin 300072,China) Abstract:Straight—run gasoline separation was studied witIl a novel column structure.the dividing wall column .This process was simulated with a commercial software HYSYS,and then the optimized design parameters were obtained.Based on these parameters,operation conditions such as the reflux ratio and the liquid sprit ratio were investigated with a pilot plant.Experimental results revealed that a higher reflux ratio is beneficial t0 the product separation,while the energy consumption is relatively higher. Also,the liquid split ratio has a wider range for selection,which is an important factor for the product quality. Key words-dividing wall column;fully thermally coupled;straight-run gasoline;distillation 精馏是化学工业过程中非常重要的分离方法, 气,图1所示的结构被认为是立板式隔板塔的典型 但最大缺点是能耗很高。随着能源危机和人

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