Al3Ti颗粒增强镁基复合材料的反应烧结.pdfVIP

学兔兔 第27卷第6期 粉末冶金技术 Vo1．27，No．6 2009年12月 Powder M etallurgy Technology Dec．2009 Al3 Ti颗粒增强镁基复合材料的反应烧结术 杨子润 王树奇一 鞠新庆 陈康敏 (江苏大学材料科学与212程学院，江苏镇江 21201 3) 摘 要： 采用Mg-Al—Ti反应体系，反应烧结制备了A1，Ti颗粒增强镁基复合材料，研究了烧结工艺对A1 Ti／ Mg复合材料的组织和密度的影响。研究结果表明：采用镁、铝和钛粉反应烧结可以获得致密的A1 Ti／Mg复 合材料，Al Ti为原位形成，呈直径为0．5～5 m颗粒状较均匀地分布在镁基体中。烧结工艺(温度和保温时 间)对 A1 Ti／Mg复合材料的组织和密度有着明显的影响，随着温度升高和保温时间延长，原位反应越完全，有 利于Al，_ri颗粒的分散，但过高温度和保温时间的延长，将造成颗粒的再团聚和镁的烧损。A1 Ti／Mg复合材 料较佳的烧结工艺参数为：温度750～8o0℃，保温时间90～120min。 关键词：复合材料；镁；反应烧结；显微组织 Reaction sintering of AI3 Ti particulate reinforced ng matrix composite Yang Zirun，Wang Shuqi，Ju Xinqing，Chen Kangmin (School of Materials Science and Engineering，Jiangsu University，Zhenjiang Jiangsu 212013，China) Abstract：A titanium tri—aluminide(A13 Ti)particulate reinforced Mg matrix composite has been fabricated through the reaction sintering of Mg—A1·Ti system．The microstructure and relative density of A13 Ti／Mg composite under the different sintering processes was investigated by using XRD and SEM．The results show that the high dense A13 Ti／Mg composite is made through the reaction sintering of Mg，A1 and Ti powders．A13 Ti particulates are in situ formed with size of 0．5—5 um and relatively homogeneously distribute in the matrix．It is found that there are significant effects of sintering processes(the temperature and holding time)on the microstructure and relative density of the composite． With the temperature and holding time increasing，in situ reaction is readily completed and A13 Ti particulates dispersed．However，excessively high temperature and long time lead t