稀土元素钇对粉末冶金制备V-5Cr-5Ti合金微观组织的影响.pdfVIP

学兔兔 第20卷第1期 粉末冶金材料科学与工程 2015年2月 Vb1．2O NO．1 Materials Science and Engineering of Powder Metallurgy Feb．2015 稀土元素钇对粉末冶金制备V．5Cr．5Ti合金 微观组织的影响 程 亮 ，李 强 ，董鲜峰 ，李启寿 ，彭丽霞 (1．中国工程物理研究院，绵阳621900；2．表面物理与化学重点实验室，绵阳621907 摘 要：采用粉末冶金方法，制各含不同质量分数钇(0％，O．5％，1％，2％)的V一5Cr-5Ti合金。利用金相显微镜、 扫描电镜(SEM)和能谱仪(EDS)等分析稀土元素钇对V一5Cr-5Ti合金显微组织的影响。结果表明添加钇能够显著改 善钒合金微观组织结构，使晶粒细化；可有效消除粗大富钛条状第二相，而析出尺寸约为3 ixm的富钇颗粒，富 钇颗粒分布于晶粒内部和晶界处，但以晶粒内部为主。 关键词：稀土钇；V．5Cr．5Ti合金；富钇相；微观组织；粉末冶金 中图分类号：TG146．4 文献标识码：A 文章编号：1673—0224(2015)1．14．05 Effect of yttrium on microstructure of V-5Cr-5Ti alloys prepared by powder metallurgy CHENG Liang ，LI Qiang ，DONG Xian-feng ，LI Qi．shou ，PENG Li。xia2 (1．Chinese Academy ofEngineering Physics，Mianyang 621900，China； 2．National Key Laboratory for Surface Physics and Chemistry，Mianyang 621907，China) Abstract：V一5Cr一5Ti alloys with various mass fraction of yttrium (O％，0．5％，1％，2％)were prepared by powder metallurgy．In order to analyse the effect of yttrium addition on microstructure of vanadium alloys，techniques of optical microscopy(OM)，scanning electron microscopy(SEM)and energy dispersive X—ray spectrometer(EDS)were applied． Results are as follows：rare—earth yttrium shOWS great affect on the microstructure of vanadium alloys．The addition of yttrium can refine the grain size，and eliminate the strip sharped Ti—enriched second phases effectively．Instead，yttrium- enriched phases with sizes of about three micrometers are formed mostly inside the grains，and also in the grain