阳极溶出伏安法与石墨炉原子吸收光谱法在血铅检测中的应用比较_李筱薇.pdf

36 　 1 　　　 Vol.36　No.1 9　　　0 2007 　1 JOURNAL OF HYGIENE RESEARCH 　　　 Jan.　2007 :1000-8020 (2007)01-0090-03 ·· 李筱薇　高俊全 , 　100050 :　比较评价阳极溶出伏安法与石墨炉原子吸收光谱法在血铅检 中的应用, 评价2 种方法的 实用性和可靠性。 　分别运用2 种方法对3 种血液样品(牛血、大鼠血和人血)同时进行检 , 检 结果 采用统计学分析。 　阳极溶出伏安法和石墨炉原子吸收光谱法 定血铅的最低检 限分别为 5.3 μg L 和0.045μg L;定量限分别为17.8μg L 和 0.15μg L。 2 种方法 定3 种血液样品, 结果经t 检验, P0.05, 呈 高度相关。 　石墨炉原子吸收光谱法灵敏度高于阳极溶出伏安法, 2 种方法检验结果呈高度相关;阳极 溶出伏安法稳定性强, 仪器设备价廉, 操作简单, 更适用于临床大批量样品的检验。 :阳极溶出伏安法　石墨炉原子吸收光谱法　血铅检 :R446.11　R994.6　R595.2　　　　　　:B Comparisonbetween anodic strippingvoltammetry and graphite furnace atomicabsorption spectrophotometry forbloodlead analysis LI Xiaowei, GAO Junquan Institute fo Nut ition and Food Safety, Chinese Cente fo Disease Cont ol and P evention, Beijing　100050, China Abstract:Objective　To compa e and evaluate anodic st iping voltammet y (ASV)with g aphite fu nace atomic abso ption spect ophotomet y (GFAAS)fo blood lead analysis. ethods　These two methods we e used to analyze same samples of th ee kinds of blood (cattle blood, at blood human blood)at the same time.The p acticability and eliability of the esults we e evaluated by the statistic analysis.Results　Limits of detection (LOD)fo ASV and GFAAS we e 5.3μg L and 0.045μg L.Limits of quality (LOQ)we e 17.8μg L and 0.15μg L fo ASV and GFAAS.The esults that th ee kinds of blood samples we e analyzed by these two methods we e in high co elation afte t test (P 0.05). Conclusion　The data demonst ated