人工合成锆石Lu_Hf同位素标样方法研究_陈开运.pdf

31 　2 　　　　　　 Vol.31, No.2:279～288 2012 3 　　 ACTA　PET ROLOGICA　ET　MINERALOGICA 　　　　　　　Mar., 2012 ·方法与应用· Lu-Hf 1 1, 2 1 1 1 1 陈开运 ,袁洪林 , 包志安, 范　超,柳小明,宋佳瑶 (1. , , 　710069;2. , 　430074) 　:。, , Hf、Lu、Yb、 、Th、Pb , , 。 Lu-Hf , Lu、Yb、 、Th、Pb , Hf Lu-Hf 。 :;Lu-Hf ;;;LA-MC-ICPMS :P599　　　　　　　　:A 　　　　　　　　:1000-6524(2012)02-0279-10 A preliminary study of the method for synthetic zircon Lu-Hf isotopic standard 1 1,2 1 1 1 1 CHEN Kai-yun , Y AN Hong-lin , BAO Zhi-an , FAN Chao , LI Xiao-ming and SONG Jia-yao (1.State Key Laboratory of Continental Dynamics, Department of Geology, Northwest niversity, Xian 710069, China ; 2.State Key Laboratory of Geological Processes and Mineral Resources, Faculty of Earth Sciences, China niversity of Geosciences, Wuhan 430074, China) Abstract :This paper studies the experimental conditions, composition, trace element content and Lu-Hf isotopic ratios in synthetic zircons.The authors used zirconia and lithium silicate as raw material and lithium molybdate and molybdenum oxide as flux, added such elements as Hf, Lu, Yb, , Th, and Pb, and then transferred to the platinum crucible with lid after full mixing.In the high-temperature muffle furnace, they were heated at 950℃continuously for growth of zircon crystals.The synthetic zircon is a good tetragonal crystal and has the same Raman spectra as the standard type of zircon crystals.Laser ablation system with inductively coupled plas- ma mass spectrometry (LA-ICP-MS)was used to measure the content of trace elements in syntheticzircon, and Lu-Hf isotopic ratios were determined by LA-MC-ICPMS.The results show