DZ125高温合金过冷凝固晶粒细化机制研究.pdfVIP

学兔兔 Jul。2009 铸 造 VOI．58 NO．7 FOUNDRY ·677· DZ1 25高温合金过冷凝固晶粒细化机制研究 周 俊 ，谢发勤 ，吴向清-，张 军 (1．西北工业大学航空学院，陕西西安710072；2．西北工业大学凝固技术国家重点实验室，陕西西安710072) 摘要：采用熔盐净化剂与循环过热相结合的方法，对DZI25高温合金晶粒细化机制进行了系统研究。在所获得过冷度 范围内 ( !8OK)，发现两次晶粒细化，第一次产生于48～85K，第二次产生于临界过冷度160K之后。枝晶生长理论 指出，枝晶重熔大小可以用无量纲过热度来衡量，无量纲过热度随过冷度的增大先增加后减小。理论计算和试验结果 表明，小过冷下晶粒细化是由枝晶熟化重熔引起，大过冷下晶粒细化是枝晶破碎再结晶所致。 关键词：DZ125高温合金；过冷；晶粒细化；再结晶 中图分类号：TG132．3 文献标识码：A 文章编号：1001—4977(2009)O7—0677—04 Research On GOn rain Refinement Mechanismanis ofoT Undercooled Solidified DZ1 25 Superalloy ZHOU Jun1，XIE Fa．qin1．2，WU Xiang．qing’，ZHANG Jun (1．SchooI of Aeronautics，Northwestern Polytechnical University，Xi。an 71 0072，Shaanxi，China； 2．State Key Laboratory of Solidification Processing。Northwestern Polytechnical University， Xi。an 71 0072，Shaanxi，China) Abstract：The grain refinement mechanisms of undercooled DZ1 25 superalloy melt were systemati- cally investigated by the method of molten salt purification combined with cycled superheating． Within the achieved range of undercoolling 0-1 80 K．there were two processes of grain refinements in the alloy．ORe took place in the undercooling range of 48．85 K．and the other beyond the critical undercooling 1 6O K．Based on dendrite growth theory．the tendency of the dendrite remelting can be evaluated with the dimensionless superheating． With the increase of undercooling，the dimensionless superheating increases first and then decreases．Both theoreticaI calculations and experimental observations indicate that the grain refinement at lOW und