检测限、最小检测浓度等概念的定义及比拟(国外英文资料).docVIP

检测限、最小检测浓度等概念的定义及比较(国外英文资料) But also is limited by a blank background absolute level, only when the signal noise ratio and blank background to a certain extent can reliably distinguish and detected. The higher the noise and blank background, the higher the actual measured concentration, indicating that high noise and blank background values will make the test limits worse. Detection limit refers to produce a reliable can be required for the analysis of the detection signal of a certain element of the minimum concentration or content, and the determination limit is specified amount limit that can be achieved in actual analysis. Because when the content of elements in the sample is equivalent to the method detection limit, although can reliably detect the signal analysis, proves that the elements in the sample do exist, but quantitative measurement error can be very big, the results of the measurement have only the value of qualitative analysis. The determination limit should always be above the check limit. But in IUPAC1997 through the analysis of the term outline of [30], determination limit (determination limit, limit of determination) renamed the loq (quantification limit, 18.4.3.7) or minimum quantitative value (minimum quantifiable value, 18.4.3.7). The definition and comparison of test limits, minimum test concentration and other concepts United States national bureau of standards The definition of the lower limit is chaotic, and some people think that the lower limit is the minimum (or the lowest concentration) of the method, and the calculation method is inconsistent; The instrument manufacturer thinks that the noise level of the instrument should be used to indicate the lower limit. Some people think that analyzing the gap means that trace analysis is more reasonable. The national bureau of standards (NBS) has the following three types: The instrument detects the lower limit That is, the reliable minimum signal for instrument detection, relative to the back