牡蛎钙英文检方法OYSTER 40.docVIP

CALCIUM CARBONATE OYSTER 40% IDENTIFICATION It gives the reaction of carbonates (2.3.1). weighs approximately 100 mg of sample and transfer to a test-tube of 20ml add 2ml of purified water and stirring until a suspension add 3 ml of dilute acetic acid solution, and Close the tube immediately using a stopper fitted with a glass tube bent twice at right angles. the solution must become effervescent and gives off a colourless and odourless gas. Heat gently and collect the gas in 5 ml of barium hydroxide solution A white precipitate is formed that dissolves on addition of an excess of hydrochloric acid 0.2 ml of solution S gives the reactions of calcium (2.3.1). Solution S: 1. Accurately weigh 5.0g of sample and transfer to a 100ml beaker 2. Add 80ml of diluted acetic acid solution, and mix 3. When effervescence ceases, heat the solution to boil for 2 minutes 4. Cool to room temperature, 5. Transfer all the solution to a volumetric flask 100.0ml 6. Dilute with dilute acetic acid solution to 100ml, and mix 7. If necessary, filter the solution through a sintered-glass filter. 朗读 显示对应的拉丁字符的拼音 ? 字典 - 查看字典详细内容 介词 to in at with 代词 it you ye 冠词 the Test – Method A Transfer 0.2ml of solution S to a test tube of 20ml add 0.5 ml of a 2 g/l solution of glyoxal-hydroxyanil R in alcohol R, 0.2 ml of dilute sodium hydroxide solution R and 0.2 ml of sodium carbonate solution R, mix add 1 ml to 2 ml of chloroform R, and stir add 1 ml to 2ml of purified water, and stir again. The chloroform layer is coloured red. Test –Method B Transfer 0.2ml of solution S to a test tube of 20ml Add 0.5 ml of potassium ferrocyanide solution R. and mix The solution remains clear. Add about 50 mg of ammonium chloride R. and mix A white, crystalline precipitate is formed. TESTS Solution S. Dissolve 5.0 g in 80 ml of dilute acetic acid R. When the effervescence ceases, boil the solution for 2 min, allow to cool, dilute to 100 ml with dilute acetic acid R and filter, if necessary, through a s