试验一 葡萄糖的性状、辨别和检查2008级(国外英文资料).docVIP

实验一 葡萄糖的性状、鉴别和检查2008级(国外英文资料) The amount of water added to the water is dissolved and diluted to the scale (SO42 - that is equal to 100 mu g per 1ml). 6, 25% BaCl2: take BaCl2250g and add water to dissolve 1L. Ammonium thiocyanate solution: ammonium thiocyanate 30g, plus water to dissolve 100ml. 8, standard iron solution: precision according to 0.863 g, ammonium ferric sulfate 1 l bottle, add water dissolves, add 2.5 ml of sulfuric acid diluted to scale, shake well, as a reserve liquid. Prior to use, the precise amount of the storage liquid 10ml, in a 100ml bottle, the addition water is diluted to the scale and shake well, which is equal to the standard solution of 10 mu g Fe per 1 ml. 9, acetate buffer (pH = 3.5) : 25 g ammonium acetate, 25 ml water dissolves, add 7 38 ml, mol/l HCL solution with 2 mol/l HCL solution or 5 mol/l ammonia solution accurately adjust pH 3.5 (potential method instruction), diluted to 100 ml. 10, 7 molar hydrochloric acid: 630ml of hydrochloric acid, plus water to dissolve 1000ml. 2 molar hydrochloric acid: 180ml of hydrochloric acid, plus water to dissolve 1000ml. Thioacetamide test liquid: take thioacetamide 4g, add water to dissolve 100ml, keep it in the refrigerator, call it solution A; 1 mole/l hydroxide solution 15ml, water 5.0 ml and glycerol 20ml composed of solution B; Before using, remove the solution B5.0 ml, add solution A1.0 ml, heat the water bath for 20 seconds, cool and use immediately. Standard lead solution: it is called the nitric acid lead 0.160 g, in 1000ml flask, after 5ml of nitric acid and 50ml water, dilute the water to the scale and shake well as a reservoir. Prior to use, the precise amount of the storage liquid 10ml, in a 100ml bottle, the water is diluted to the scale and shake well, which is the equivalent of 10 mu g of Pb standard solution per 1 ml. Dilute sulfuric acid: 57ml of concentrated sulphate, diluted to 1000ml. This liquid contains H2SO4 for 9.5% ~ 10.5%. Potassium bromide test solution: take br