岩石碳酸盐含量的测定(国外英文资料).docVIP

岩石碳酸盐含量的测定(国外英文资料) China university of petroleum (petrophysics) laboratory report Experiment date: 2011.10.28: Class:09131503: zhang yan bin The determination of the carbonate content of rocks One. The purpose of the experiment Deepen understanding of the concept and meaning of carbonate content. Master the principle and method of measuring carbonate content. Two. Experimental principle The carbonate rocks in the rock are mainly calcite (CaCO3) and dolomite (CaMg (CO3) 2). The reaction vessel volume must be, a certain amount of rock sample and sufficient amount of dilute hydrochloric acid reaction, produce CO2 gas, the pressure increase in the container. The equation is as follows: CaCO3 + HCL = 2 H2O + CaCl2 + CO2 write CaMg (CO3) 2 + 4HCl = 2H2O + CaCl2 + MgCl2 + 2CO2 arrow The more carbonate in the sample, the greater the pressure of CO2 in the container. To a certain quality of pure calcium carbonate and a certain quality of sample with plenty of dilute hydrochloric acid respectively after the reaction of CO2 gas pressure, can calculate the samples contained carbonate content. The formula is as follows: The mass of pure calcium carbonate, g; Sample mass, g; - a percentage of the mass of carbonate in the sample. - the pressure after the pure calcium carbonate and rock sample reactions, kPa. Three. Experimental process and equipment (a) flow chart GMY tester - Ⅱ carbonate content (b) control panel Four. Step by step Use the sample umbrella to claim about 0.2 grams of pure calcium carbonate. Place the sample umbrella under the cover of the reaction room and resist with the top lever. Take 20ml and 5% of the diluted hydrochloric acid in the reaction cup, and place the reaction cup in the holder, turning the t-handle to seal it. Close the release valve and record the initial pressure readings. 5. Pull the plunger to make the sample umbrella plunged into the reaction chamber, make pure calcium carbonate and hydrochloric acid reaction, after being pressure s