氮测定法(国外英文资料).docVIP

氮测定法(国外英文资料) Hangzhou kangembei pharmaceutical co., LTD. Number: stp-ca-036-01 Nitrogen determination method Make up Trial nucleus Trial order approval Date of the year Date of the year Date of the year Date of the year distribution Quality department (1), laboratory (1) perform Date of the year Number of pages A total of 2 pages copy 2 Eye: standard operation of nitrogen determination Fan: the nitrogen test Job responsibility: The QC inspector is responsible for testing the sample according to the standard The QC supervisor is responsible for the drafting of this standard and is responsible for the inspection report issued In: 1. A brief introduction Chinese pharmacopoeia is suitable for determination of nitrogen content containing nitrogen organic matter. 1.2 this law department will test samples under the action of sulfuric acid and catalyst, the thermal decomposition of the transformation of organic nitrogen to ammonium sulfate, then through alkali ammonia distillate and alkaline absorption boric acid solution, the titration with sulfuric acid droplets, and the nitrogen content. Briefly describe the three steps of digestion, distillation and titration. The determination of the first step (the constant method) and the second (semi-minor) method shall be chosen according to the provisions under the category and the specific tests. Instruments and drugs 2.1 the instrument The 2.1.1 constant determination nitrogen is composed of 500ml KMS flask, nitrogen balls and condensation tubes. The 2.1.2 and a half trace determination of the nitride is composed of 1000ml round bottom flask, a distiller with nitrogen ball, and a straight condenser tube. Analytical balance: a scale of 0.1 mg, suitable for precise measurement of 0.1 g. A balance of 0.01 mg is applied to the precision weighing 0.1 g. 2.1.4 digestion application adjustable voltage furnace heating. The distillate can be heated by adjustable voltage or electric heating. Use the latex pipe or rubber hose of the 2.1.5