膜在乳制品中的应用及相关文献.ppt

膜在乳制品中的应用及相关文献 背景，优缺点 膜分离方式，牛乳加工 膜在乳制品中的应用 实验方法及结论 膜应用概述 牛乳与膜分离 膜的选择 实验内容 膜在乳制品中的应用及 膜在乳制品中的应用背景 背景： 20世纪70盔[E代初．国外开始了超滤和反渗透用于乳品加工的研究。 直到1974年，找到了有效减少膜污染并进行清洗．使之透量恢复到初始水平的方法后。膜技术迅速地实现了产业规模的应用。 至20世纪90年代中期已普遍广泛使用．其中用于乳品工业的膜技术包括微滤、超滤、纳滤和反渗透。 膜法加工的优势 用膜分离技术不仅可以最大程度截流活性蛋白质．还能保留奶中原有的风味物质 降低生产成本，及综合利用副产品，实现无污染排放等环保要求 1.高温操作，2.破坏风味、营养 3.杀死的细菌体残留在牛奶中 巴氏杀菌或超高温瞬时灭菌缺点 膜分离方式 3.纳滤：主要用于乳清的部分脱盐。 牛乳加工及膜的选择 乳清蛋白分离、脱盐及乳糖 浓缩 牛乳冷杀菌 各种牛乳制品加工过程 牛乳浓缩 提取牛乳活性成分（乳铁蛋白、免疫球蛋白） 膜的选择 Text in here 牛乳浓缩： 乳清 蛋白质浓缩液 0.07到0.7MPa 乳糖、非蛋白质、乳酸、盐类 乳糖浓缩液 7.14MPa 低BOD废水 UF RO 2、乳清蛋白分离、脱盐及乳糖浓缩 3、冷杀菌 稀奶油 截留液 Materials Materials: WPC (the powder contained 82% protein), TFA, ACN, HC,H3PO4, NaOH Membrane riga :Pellicon 2 mini cassette holder A GJ series 120 pump 1 L jacketed glass tank reactor A thermostatic water bath Two different polyethersulfone (PES) membranes: PES1 and PES5 , each with a filtration area of 0.1 m2 methods Analytical methods Hydrolysates, retentates and permeates chromatographic profiles were obtained using a Jupiter C18 (5μm, 4.6*150 mm) column, installed within a highperformance liquid chromatograph (HPLC) Agilent 1200 series. WPH peptides Trobs and Trtheo values across the PES5 membrane WPH peptides Trobs and Trtheo values across the PES1 membrane Results 1. If comparing Figs, it is interesting to note that, even though the membranes markedly different NMWCO, the peptides transmitted across them were almost the same. 2. Their MW is not exactly representative of their real size or shape. 3. peptides Trobs was different (higher or lower) than the Trthe, and that it varied with pH. 4. The neutral peptides Trobs were pH6pH8pH2. The basic peptides Trobs were pH8pH6pH2, the acidic peptides were always rejected. Separation factors and membranes performance Conclusions PES5 membrane was preferred due to its higher S and peptide Tr.