一种橘皮精油洗涤液的工艺放大研究.pdfVIP

2015 年第24 期 广东化工 . 16 . 第42 卷总第314 期 一种桶皮精油洗涤液的工艺放大研究 韩杰， 彭威，吴春阳， 花儿 [摘 要]原先研制的含横皮精泊绿色洗涤液工艺单位最为 l ∞mL时的缘佳配比为D-拧橡烯 15%. AEO-714%. AES 8%. 乙醉 8%. 拧橡酸纳2%. KCI 0.25 %.余量为蒸馆水. 为了研究该洗衣液的工艺放大，本研究以 10∞mL为单位配和l簸，以去污效率为参考指标.通过正 交试验获得了其最佳配比为: D-拧橡烯 15 %. AEO-7 14 %. AES 8 %.乙醇 8%. 拧核酸纳2 %. KCI 0.25 %.余.最为盖在tæ水.与 IOO mL为单 位盘时的最优配比相同.通过验证试验测定了最优配比下的绿色洗涤液对汹溃的去污效率为93 %. 与 LB 洗衣液的去污比值为1.03: 对炭 黑污垢的去污效率为 61 %. 与 LB 洗衣液的去污比值为1.60. 本研究中洗涤污布片时采取直接将搅拌捧放入洗涤瓶中咆动搅挤，去污效果更佳 明显. 该洗衣浓的pH 为 7.29. 乳化及发泡能力均相当于 LB 洗衣液.本研究为该洗衣液的工艺放大研究做出了1在耍的研究基础. [关键词) 绿色洗涤液:揭皮精泊: D-拧穰烯: 工艺放大:去污效率 [中图分类号)TQ649.6 [文献标识码)A [文章编号)1 ∞7-1865(2015)24-0016-02 The Scale-up Study on a Detergent using Orange Peel Essential Oil HanJ妃. Peng Wei , Wu Chunyang, Hua Er (School ofChemistry and Chemical Engineering, Bcifang University ofNationalities, Yinchuan 750021 , China) Abstract: The small-scaled (1 00 mL) gr四n detergent including orange peel essential oil was prepared previously. Its optimum recipe ratio is D-limonene 15 %. AEO-7 14 %, AES 8 %, ethanol 8 %, sodium citrate 2 %. KCI 0.25 %, and the other was distilled water. I.n this study, in order to study the scale-up pr刷:ess. the larger-scaled (1000 mL) green detergent was prepar，创 and its delergency and the other properties were measured. Orthogonal array desi伊 experiment was employed 10 get the optimum recipe ratio for the green detergenl according 10 the optimum recipe ratio ofthe small scaled detergent. The optimum recipe ratio of the larger- scaled detergent is D-limonene 15 %. AEO-7 14 %, AES 8 %. ethanol