丙烯酸精制工艺流程(国外英文资料).doc

丙烯酸精制工艺流程(国外英文资料) 1 process Production process principle This position is responsible for acrylic from former post about 48 ﹪ (wt) of the acrylic acid aqueous solution after dehydration, acetic acid, and restructuring of the refined into 99.5 (wt) acrylic acid of high purity products. Production process flow statement 1.2.1 light component fractionation system 2 t ‐ 201 (thick acrylic jar) of acrylic acid aqueous solution by 2 p ‐ 201 a/B (acrylic charging pump) to send to 2 c ‐ 210 15 boards (fractionator light component). In this case, control and loading are controlled using FC ‐ 2032 and FC ‐ 2031. 2C ‐ 210 is the plate-type tower, with 17 panels and the upper layers of stuffing. In 2C 210, water and acetic acid are separated from acrylic by means of azeotropic distillation. The azeotropic agent is toluene. Water, acetic acid, and toluene as azeotrope by vacuum distillation from 2 c ‐ 210 top steamed, steaming from the 2 e ‐ 212 (2 c ‐ 210 overhead condenser) by CTW partial condensation, condensate into 2 d ‐ 211 (2 c ‐ 210 tower tank), no condensate gas into 2 e ‐ 213 emissions (2 c ‐ 210 tower air condenser) by CTW further condensation, condensate into the 2 d ‐ 211, also from 2 e ‐ 213 out of the non-condensable gas by water ring vacuum pump 2 p ‐ 216 a/B (2 c ‐ 210 vacuum pump) by 2 pd ‐ 216 (2 p ‐ 216 empty cans recycling tank) by 2 e ‐ 216 216 gas condenser (2 p ‐) non-condensable gas discharge the waste incineration system (U ‐ 600). In this case, the 2D ‐ 211 gas phase pressure is controlled by using PC ‐ 2002 to adjust the circulation volume. 2D: 211 is divided into two zones: water phase and toluene. The inflow of condensate is layered in the water phase, and the upper layer of toluene is flooding the toluene region. The toluene in the area of toluene is delivered from 2P ‐ 211A/B (c) 211A/B (c), which is controlled by 2FC ‐ 2003 control from 2C to 210 to the tower. The other way was to control the level of the toluene region by LC ‐ 2003 to 2T ‐ 202 (