辉钼矿在微波场中的升温特性及焙烧测试.docxVIP

PAGE \* MERGEFORMAT12 辉钼矿在微波场中的升温特性及焙烧测试 蒋永林，刘秉国项目基金：国家高技术研究发展计划项目（863计划）（项目编号：2011A064003）；国家自然科学基金项目（编号；云南省应用基础研究重点项目（编号：No. 2016FA023）。 作者简介：蒋永林（1991 - ），男，硕士研究生，主要从事微波冶金及钼冶金研究工作。 通讯作者：刘秉国，男，博士，教授；Email：bingoliu@126.com ，彭金辉，张利波，陈林 昆明理工大学冶金与能源工程学院，云南 昆明650093 昆明理工大学非常规冶金省部共建教育部重点实验室，云南 昆明650093 微波能工程应用及装备技术国家地方联合工程实验室，云南 昆明650093 摘 要：本文考察了辉钼矿在微波场中的升温行为，探究了物料量、物料厚度以及微波功率对辉钼矿升温行为的影响。研究结果表明，辉钼矿具有良好的微波吸收性能，其升温过程可分为3个阶段；物料在微波场中升温与微波功率呈正比，而与物料厚度和物料量成反比。在本试验范围内，微波功率0.5kW条件下，18 min后可将130g辉钼矿加热至800℃。从对焙烧产品进行的表征结果可知，本试验得到特征良好的的焙烧产品；微波氧化焙烧辉钼精矿制备高纯度三氧化钼是可行的。 关键词：辉钼矿；微波；升温行为；三氧化钼 The temperature rise behavior and boasting test of molybdenite in microwave fields Jiang yonglin, Liu bingguo, Peng jinhui, Zhang libo, Chen lin Faculty of Metallurgical and Energy Engineering, Kunming University of Science and Technology, Kunming 650093, Yunnan, China Key Laboratory of Unconventional Metallurgy, Ministry of Education, Kunming University of Science and Technology, Kunming 650093, Yunnan, China National local joint engineering laboratory of engineering Applications of Microwave Energy and Equipment Technology, Kunming 650093, Yunnan, China Abstract: Temperature rising behavior of molybdenite was investigated in fields of microwave. The effect of materials thickness, materials quality and microwave power on temperature were discussed. The results showed that molybdenite had good microwave absorption properties, the heating process can be divided into three phases. Temperature rising of molybdenite in the microwave field was found in a positive relationship with microwave power, while negative with both material thickness and material mass within the experimental ranges. In 0.5kW microwave power, the temperature of molybdenite specimen with the quality of130g can rise from room temperature up to 800℃ until 18 min. The roasting product was examined by X-ray Diffraction and Scanning Electron Microscope, which indicates that good performance MOO3 was produced in the exp