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甲缩醛甲醇分离之萃取精馏与变压精馏的设计与控制
ABSTRACT
In this paper, two methods for methylal/methanol separation is presented using
extractive distillation (ED) and fully heat integrated pressure swing distillation (PSD).
Rigorous steady state and dynamic simulations for this neat operation are
implemented on commercial simulators (Aspen Plus and Aspen Dynamics). For ED,
N,N-dimethylformamide was selected as an suitable entrainer by comparing infinite
dilution relative volatilities. On the basis of global economic optimization, a design
with optimized operation conditions for this process is developed. For dynamic
simulations, feed flow rate and feed composition disturbances are used to evaluate the
dynamic performance of several control structures. The results reveal that the control
structure with fixed reflux ratio can handle all disturbances well, except one kind of
composition disturbance. An improved control structure with R/F ratio scheme is used
to maintain the two products purity requirements. Dynamic simulation results reveal
that this control structure can handle feed flow rate and composition disturbances
quite effective. For PSD, based on the proposed partially optimization and global
economical optimization, an optimized configuration for this fully heat integrated
pressure swing distillation is developed. Several control structures for this fully heat
integrated pressure swing distillation system are presented. The dynamic simulation
results reveal that the proposed basic control structure is unable to maintain the two
bottom product at their quality specification. This problem can be resolved by using a
pressure-compensated temperature control scheme. The dynamic responses show that
this control structure works pretty well for this fully heat integrated pressure swing
distillation, even for la
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