有机粘土矿物的制备选读.docVIP

XXX大学 毕业设计（论文） 题 目： 有机粘土矿物的制备 学 院： 专业班级： 指导教师： 职称： 学生姓名： 学 号： 摘 要 季铵盐杀藻剂是人们当前研究赤潮防治剂的热点之一，季铵盐类化合物是一类价廉的工业产品。本文通过实验制备了经十六烷基三甲基溴化铵有机改性的蒙脱土，发现在反应温度为30℃，pH=7,反应时间为4h，放置时间为1h时的有机改性蒙脱土的有机改性效果最好，且1.0CEC的有机改性蒙脱土的稳定性最好。通过控制相同条件下不同温度，不同pH，不同反应时间，不同CEC，和不同放置时间的有机改性蒙脱土，来通过重铬酸钾容量法-稀释热法测定土样有机质的含量的变化量，以找出制备十六烷基三甲基溴化铵有机改性蒙脱土的最佳温度，最佳pH，最佳反应时间和稳定性最佳的CEC，及最佳放置时间。通过改性有机蒙脱土去除赤潮藻实验，我们可以看到不同CEC的有机改性蒙脱土，在不同条件下的除藻率也不尽相同。结果表明经过少量十六烷基三甲基溴化铵改性的蒙脱土的除藻率远远大于原土的除藻率。 关键词：有害赤潮,季铵盐,蒙脱土，有机改性 ABSTRACT Organic algicides study is one of the hot that people study how to control agent of red tide.The quaternary ammonium compounds are a class of inexpensive industrial products. This experiment has prepared organically montmorillonite modified by cetyl trimethyl ammonium bromide, and found that when the temperature is 30 ℃, pH is 7, the reaction time is 4h, and placing time is 1 hour after the montmorillonite is organically modified,the organically modified montmorillonite has the best effect, at the same time, the stability of montmorillonite of 1.0CEC is the best. Through the control of different temperatures, different pH, different reaction time ,different CEC,and different storage time of organic modified montmorillonite under the same conditions, measures the changes in soil organic matter content to find the optimal temperature for preparing cetyl trimethyl ammonium bromide organically modified montmorillonite, the best pH, reaction time and stability best best CEC, and the best placing time by the thermal dilution method of potassium dichromate volumetric method.By using the modified montmorillonite experiments to remove algae, we can see that removal efficiency of the organic modified montmorillonite